(+/-)-1-(4-benzyloxyphenyl)-7-(2-benzyloxy-3,4-dimethoxyphenyl)heptan-3-ol

Base Information

• Chemical Name: (+/-)-1-(4-benzyloxyphenyl)-7-(2-benzyloxy-3,4-dimethoxyphenyl)heptan-3-ol
• CAS No.: 68486-78-2
• Molecular Formula: C₃₅H₄₀O₅
• Molecular Weight: 540.7

Synonyms:(+/-)-1-(4-benzyloxyphenyl)-7-(2-benzyloxy-3,4-dimethoxyphenyl)heptan-3-ol

Chemical Property of (+/-)-1-(4-benzyloxyphenyl)-7-(2-benzyloxy-3,4-dimethoxyphenyl)heptan-3-ol

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of (+/-)-1-(4-benzyloxyphenyl)-7-(2-benzyloxy-3,4-dimethoxyphenyl)heptan-3-ol

There total 14 articles about (+/-)-1-(4-benzyloxyphenyl)-7-(2-benzyloxy-3,4-dimethoxyphenyl)heptan-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

benzyl bromide (100-39-0) + 1-(4-hydroxyphenyl)-7-(2-hydroxy-3,4-dimethoxyphenyl)heptan-3-ol (68486-80-6) → (+/-)-1-(4-benzyloxyphenyl)-7-(2-benzyloxy-3,4-dimethoxyphenyl)heptan-3-ol (68486-78-2)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; In acetone; Reflux;

DOI:10.1016/j.bbrc.2020.06.122

Reference yield: 42.0%

4-(2-benzyloxy-3,4-dimethoxyphenyl)-1-bromobutane (68486-76-0) → 1-(2-benzyloxy-3,4-dimethoxyphenyl)butane (74882-17-0) + (+/-)-1-(4-benzyloxyphenyl)-7-(2-benzyloxy-3,4-dimethoxyphenyl)heptan-3-ol (68486-78-2) + 1,8-bis-(2-benzyloxy-3,4-dimethoxyphenyl)octane (74882-18-1)

Guidance literature:

With 3-(4-(benzyloxy)phenyl)propanal; magnesium; In tetrahydrofuran; for 18h; Ambient temperature;

Reference yield: 42.0%

3-(4-(benzyloxy)phenyl)propanal (68486-77-1) + 4-(2-benzyloxy-3,4-dimethoxyphenyl)-1-bromobutane (68486-76-0) → 3-[4-(benzyloxy)phenyl]propan-1-ol (61440-45-7) + 1-(2-benzyloxy-3,4-dimethoxyphenyl)butane (74882-17-0) + (+/-)-1-(4-benzyloxyphenyl)-7-(2-benzyloxy-3,4-dimethoxyphenyl)heptan-3-ol (68486-78-2) + 1,8-bis-(2-benzyloxy-3,4-dimethoxyphenyl)octane (74882-18-1)

Guidance literature:

With magnesium; In tetrahydrofuran; for 18h; Ambient temperature;

upstream raw materials:

3-(4-(benzyloxy)phenyl)propanal

4-(2-benzyloxy-3,4-dimethoxyphenyl)-1-bromobutane

1,2,3-trimethoxybenzene

3-(2-hydroxy-3,4-dimethoxybenzoyl)propionic acid

Downstream raw materials:

1-(4-benzyloxyphenyl)-7-(2-benzyloxy-5-bromo-3,4-dimethoxyphenyl)heptan-3-ol

(+/-)-1-(4-benzyloxyphenyl)-7-(2-benzyloxy-3,4-dimethoxy-5-iodophenyl)heptan-3-ol

(+/-)-1-(4-benzyloxy-3-iodophenyl)-7-(2-benzyloxy-3,4-dimethoxy-5-iodophenyl)heptan-3-ol

1-(4-hydroxyphenyl)-7-(2-hydroxy-3,4-dimethoxyphenyl)heptan-3-ol

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