1-acetoxy-1-(2,3,5-tribenzyloxyphenyl)propan-2-ylphosphonic bis(dimethylamide)

Base Information

Chemical Name:1-acetoxy-1-(2,3,5-tribenzyloxyphenyl)propan-2-ylphosphonic bis(dimethylamide)
CAS No.:113524-01-9
Molecular Formula:C₃₆H₄₃N₂O₆P
Molecular Weight:630.721
Hs Code.:

Synonyms:1-acetoxy-1-(2,3,5-tribenzyloxyphenyl)propan-2-ylphosphonic bis(dimethylamide)

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Chemical Property of 1-acetoxy-1-(2,3,5-tribenzyloxyphenyl)propan-2-ylphosphonic bis(dimethylamide)

Chemical Property:

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Technology Process of 1-acetoxy-1-(2,3,5-tribenzyloxyphenyl)propan-2-ylphosphonic bis(dimethylamide)

There total 4 articles about 1-acetoxy-1-(2,3,5-tribenzyloxyphenyl)propan-2-ylphosphonic bis(dimethylamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 108-24-7
acetic anhydride

: 113523-99-2
1-hydroxy-1-(2,3,5-tribenzyloxyphenyl)propan-2-ylphosphonic bis(dimethylamide)

: 113524-01-9
1-acetoxy-1-(2,3,5-tribenzyloxyphenyl)propan-2-ylphosphonic bis(dimethylamide)

Guidance literature:: In pyridine; for 16h;

Reference yield:

: 36873-96-8
2,3,5-trimethoxybenzoic acid

: 113524-01-9
1-acetoxy-1-(2,3,5-tribenzyloxyphenyl)propan-2-ylphosphonic bis(dimethylamide)

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / HCl / 4 h / Heating

2: 90 percent / 1.) buthyl-lithium/hexane / tetrahydrofuran / 1.) -50 deg C, 3 h; 2.) -78 deg C, 2 h

3: 90 percent / NaBH₄ / methanol / 1 h / 0 °C

4: 98 percent / pyridine / 16 h

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; hexane; In tetrahydrofuran; pyridine; methanol;

Reference yield:

: 110361-77-8
methyl 2,3,5-trimethoxybenzoate

: 113524-01-9
1-acetoxy-1-(2,3,5-tribenzyloxyphenyl)propan-2-ylphosphonic bis(dimethylamide)

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / 1.) buthyl-lithium/hexane / tetrahydrofuran / 1.) -50 deg C, 3 h; 2.) -78 deg C, 2 h

2: 90 percent / NaBH₄ / methanol / 1 h / 0 °C

3: 98 percent / pyridine / 16 h

With sodium tetrahydroborate; n-butyllithium; hexane; In tetrahydrofuran; pyridine; methanol;