1-acetoxy-1-(2,3,5-tribenzyloxy-6-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

Base Information

Chemical Name:1-acetoxy-1-(2,3,5-tribenzyloxy-6-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)
CAS No.:113524-03-1
Molecular Formula:C₃₆H₄₂ClN₂O₆P
Molecular Weight:665.166
Hs Code.:

Synonyms:1-acetoxy-1-(2,3,5-tribenzyloxy-6-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

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Chemical Property of 1-acetoxy-1-(2,3,5-tribenzyloxy-6-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

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Technology Process of 1-acetoxy-1-(2,3,5-tribenzyloxy-6-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

There total 5 articles about 1-acetoxy-1-(2,3,5-tribenzyloxy-6-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 113524-01-9
1-acetoxy-1-(2,3,5-tribenzyloxyphenyl)propan-2-ylphosphonic bis(dimethylamide)

: 113524-03-1
1-acetoxy-1-(2,3,5-tribenzyloxy-6-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

Guidance literature:: With sulfuryl dichloride; In diethyl ether; for 3h; Ambient temperature;

Reference yield:

: 36873-96-8
2,3,5-trimethoxybenzoic acid

: 113524-03-1
1-acetoxy-1-(2,3,5-tribenzyloxy-6-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / HCl / 4 h / Heating

2: 90 percent / 1.) buthyl-lithium/hexane / tetrahydrofuran / 1.) -50 deg C, 3 h; 2.) -78 deg C, 2 h

3: 90 percent / NaBH₄ / methanol / 1 h / 0 °C

4: 98 percent / pyridine / 16 h

5: 90 percent / SO₂Cl₂ / diethyl ether / 3 h / Ambient temperature

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; sulfuryl dichloride; hexane; In tetrahydrofuran; pyridine; methanol; diethyl ether;

Reference yield:

: 110361-77-8
methyl 2,3,5-trimethoxybenzoate

: 113524-03-1
1-acetoxy-1-(2,3,5-tribenzyloxy-6-chlorophenyl)propan-2-ylphosphonic bis(dimethylamide)

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / 1.) buthyl-lithium/hexane / tetrahydrofuran / 1.) -50 deg C, 3 h; 2.) -78 deg C, 2 h

2: 90 percent / NaBH₄ / methanol / 1 h / 0 °C

3: 98 percent / pyridine / 16 h

4: 90 percent / SO₂Cl₂ / diethyl ether / 3 h / Ambient temperature

With sodium tetrahydroborate; n-butyllithium; sulfuryl dichloride; hexane; In tetrahydrofuran; pyridine; methanol; diethyl ether;