4-phenylcyclohex-3-en-1-one ethylene glycol ketal

Base Information

Chemical Name:4-phenylcyclohex-3-en-1-one ethylene glycol ketal
CAS No.:724707-89-5
Molecular Formula:C₁₄H₁₆O₂
Molecular Weight:216.28
Hs Code.:

Synonyms:4-phenylcyclohex-3-en-1-one ethylene glycol ketal

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Chemical Property of 4-phenylcyclohex-3-en-1-one ethylene glycol ketal

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Technology Process of 4-phenylcyclohex-3-en-1-one ethylene glycol ketal

There total 8 articles about 4-phenylcyclohex-3-en-1-one ethylene glycol ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 3262-89-3
triphenylboroxine

: 4746-97-8
cyclohexanedione monoethylene ketal

: 724707-89-5
4-phenylcyclohex-3-en-1-one ethylene glycol ketal

Guidance literature:: With tetrakis(triphenylphosphine)nickel⁽⁰⁾; water; 1,2-bis-(dicyclohexylphosphino)ethane; In diethylene glycol dimethyl ether; at 110 ℃; for 24h; Glovebox; Schlenk technique; Inert atmosphere;
DOI:10.1021/jacs.7b02742

Reference yield: 68.0%

: 170011-47-9
1,4-dioxaspiro[4.5]dec-7-en-8-yl trifluoromethanesulfonate

: 724707-89-5
4-phenylcyclohex-3-en-1-one ethylene glycol ketal

Guidance literature:: With 1-methyl-pyrrolidin-2-one; iron(III)-acetylacetonate; In tetrahydrofuran; at -30 ℃; for 0.25h;
DOI:10.1021/jo0498866

Reference yield: 54.6%

: 170011-47-9
1,4-dioxaspiro[4.5]dec-7-en-8-yl trifluoromethanesulfonate

: 98-80-6
phenylboronic acid

: 724707-89-5
4-phenylcyclohex-3-en-1-one ethylene glycol ketal

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate; In 1,2-dimethoxyethane; water; at 110 ℃; for 3.5h; Inert atmosphere; Sealed tube;