rac-[1-(1-allyloxy-1-phenylmetyl)-1-vinylallyloxy]-tert-butyldimethylsilane

Base Information

Chemical Name:rac-[1-(1-allyloxy-1-phenylmetyl)-1-vinylallyloxy]-tert-butyldimethylsilane
CAS No.:292163-82-7
Molecular Formula:C₂₁H₃₂O₂Si
Molecular Weight:344.569
Hs Code.:

Synonyms:rac-[1-(1-allyloxy-1-phenylmetyl)-1-vinylallyloxy]-tert-butyldimethylsilane

Suppliers and Price of rac-[1-(1-allyloxy-1-phenylmetyl)-1-vinylallyloxy]-tert-butyldimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of rac-[1-(1-allyloxy-1-phenylmetyl)-1-vinylallyloxy]-tert-butyldimethylsilane

Chemical Property:

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Technology Process of rac-[1-(1-allyloxy-1-phenylmetyl)-1-vinylallyloxy]-tert-butyldimethylsilane

There total 3 articles about rac-[1-(1-allyloxy-1-phenylmetyl)-1-vinylallyloxy]-tert-butyldimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 292163-77-0
rac-3-(1-allyloxphenylmethyl)penta-1,4-dien-3-ol

: 292163-82-7
rac-[1-(1-allyloxy-1-phenylmetyl)-1-vinylallyloxy]-tert-butyldimethylsilane

Guidance literature:: With sodium hydride; In tetrahydrofuran; Heating;
DOI:10.1021/jo005534x

Reference yield:

: 4358-87-6
(RS)-methyl mandelate

: 292163-82-7
rac-[1-(1-allyloxy-1-phenylmetyl)-1-vinylallyloxy]-tert-butyldimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / Ag₂O / diethyl ether / 48 h / 20 °C

2: 44 percent / tetrahydrofuran; diethyl ether / 13 h / -78 - 20 °C

3: 52 percent / NaH / tetrahydrofuran / Heating

With sodium hydride; silver(l) oxide; In tetrahydrofuran; diethyl ether; 1: Etherification / 2: Grignard reaction / 3: Condensation;
DOI:10.1021/jo005534x

Reference yield:

: 114209-14-2
(1-allyloxy-1-methoxymethyl-but-3-enyl)-benzene

: 292163-82-7
rac-[1-(1-allyloxy-1-phenylmetyl)-1-vinylallyloxy]-tert-butyldimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / tetrahydrofuran; diethyl ether / 13 h / -78 - 20 °C

2: 52 percent / NaH / tetrahydrofuran / Heating

With sodium hydride; In tetrahydrofuran; diethyl ether; 1: Grignard reaction / 2: Condensation;
DOI:10.1021/jo005534x