1β-(butan-3-one)-menthone

Base Information

Chemical Name:1β-(butan-3-one)-menthone
CAS No.:37842-16-3
Molecular Formula:C₁₄H₂₄O₂
Molecular Weight:224.343
Hs Code.:

Synonyms:1β-(butan-3-one)-menthone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1β-(butan-3-one)-menthone

Chemical Property:

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Technology Process of 1β-(butan-3-one)-menthone

There total 7 articles about 1β-(butan-3-one)-menthone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 38230-41-0
(2R)-2r-methyl-5t-isopropyl-1-hydroxymethylene-cyclohexanone-⁽⁶⁾

: 78-94-4,25038-87-3
methyl vinyl ketone

: 37842-16-3
1β-(butan-3-one)-menthone

Guidance literature:: With triethylamine; at 0 - 20 ℃; for 72h; Inert atmosphere;
DOI:10.1021/acs.orglett.0c00109

Reference yield: 32.0%

: 10458-14-7,14073-97-3,17627-49-5,7786-64-3
(2R,5S)-menthone

: 43209-86-5
3-trimethylsilyl-3-buten-2-one

: 37842-16-3
1β-(butan-3-one)-menthone

Guidance literature:: With diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; at -78 - 0 ℃;
DOI:10.1016/S0040-4020(99)00986-2

Reference yield:

: 10458-14-7,14073-97-3,17627-49-5,7786-64-3
(2R,5S)-menthone

: 37842-16-3
1β-(butan-3-one)-menthone

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / diethyl ether / 2 h / -78 °C / Inert atmosphere

1.2: 3 h / -78 °C / Inert atmosphere

2.1: triethylamine / 72 h / 0 - 20 °C / Inert atmosphere

With triethylamine; lithium diisopropyl amide; In diethyl ether;
DOI:10.1021/acs.orglett.0c00109