2,2-Dimethyl-1,3-propanediol dicarbamate

Base Information

• Chemical Name: 2,2-Dimethyl-1,3-propanediol dicarbamate
• CAS No.: 1471-52-9
• Molecular Formula: C₇H₁₄N₂O₄
• Molecular Weight: 190.199
• Hs Code.: 2924199090
• Mol file: 1471-52-9.mol

Synonyms:1,3-Propanediol,2,2-dimethyl-, dicarbamate (9CI); Carbamic acid, 2,2-dimethyltrimethylene ester(6CI,7CI,8CI); Dimebamate; Neopentyl glycol dicarbamate

Chemical Property of 2,2-Dimethyl-1,3-propanediol dicarbamate

Chemical Property:

• Vapor Pressure: 2.36E-07mmHg at 25°C
• Boiling Point: 422.7°C at 760 mmHg
• Flash Point: 247.2°C
• PSA: 106.62000
• Density: 1.2g/cm³
• LogP: 1.23080

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2-Dimethyl-1,3-propanediol dicarbamate

There total 3 articles about 2,2-Dimethyl-1,3-propanediol dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phosgene (75-44-5) + 2,2-Dimethyl-1,3-propanediol (126-30-7) → 2,2-Dimethyl-propandiol-(1,3)-dicarbamat (1471-52-9)

Guidance literature:

With antipyrine; chloroform; toluene; und Behandeln der Reaktionsloesung mit Ammoniak;

DOI:10.1021/ja01156a086

Reference yield:

2,2-Dimethyl-1,3-propanediol (126-30-7) + phenyl chloroformate (1885-14-9) → 2,2-Dimethyl-propandiol-(1,3)-dicarbamat (1471-52-9)

Guidance literature:

Multistep reaction; (i) Py, (ii) liq. NH₃;

DOI:10.1021/jm00329a012

Reference yield:

→ 2,2-Dimethyl-propandiol-(1,3)-dicarbamat (1471-52-9)

Guidance literature:

/BRN= 605291/, CO(NH2)2*HNO3/DMF;

upstream raw materials:

phosgene

2,2-Dimethyl-1,3-propanediol

phenyl chloroformate

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