p-tolyl 2,3,6-tri-O-trimethylsilyl-4-O-(2,3,4,6-tetra-O-trimethylsilyl-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:p-tolyl 2,3,6-tri-O-trimethylsilyl-4-O-(2,3,4,6-tetra-O-trimethylsilyl-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside
CAS No.:1372767-22-0
Molecular Formula:C₄₀H₈₄O₁₀SSi₇
Molecular Weight:953.765
Hs Code.:

Synonyms:p-tolyl 2,3,6-tri-O-trimethylsilyl-4-O-(2,3,4,6-tetra-O-trimethylsilyl-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-tolyl 2,3,6-tri-O-trimethylsilyl-4-O-(2,3,4,6-tetra-O-trimethylsilyl-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

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Technology Process of p-tolyl 2,3,6-tri-O-trimethylsilyl-4-O-(2,3,4,6-tetra-O-trimethylsilyl-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

There total 1 articles about p-tolyl 2,3,6-tri-O-trimethylsilyl-4-O-(2,3,4,6-tetra-O-trimethylsilyl-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: p-tolyl 2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 1372767-22-0
p-tolyl 2,3,6-tri-O-trimethylsilyl-4-O-(2,3,4,6-tetra-O-trimethylsilyl-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1002/ejoc.201101267

Reference yield:

: 1372767-22-0
p-tolyl 2,3,6-tri-O-trimethylsilyl-4-O-(2,3,4,6-tetra-O-trimethylsilyl-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

: 108-24-7
acetic anhydride

: 1372767-24-2
p-tolyl 6-O-acetyl-2,3-di-O-trimethylsilyl-4-O-(6-O-acetyl-2,3,4-tri-O-trimethylsilyl-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; acetic acid; In dichloromethane; at 20 ℃; for 48h; regioselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201101267

Reference yield:

: 1372767-22-0
p-tolyl 2,3,6-tri-O-trimethylsilyl-4-O-(2,3,4,6-tetra-O-trimethylsilyl-α-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

: 100-52-7
benzaldehyde

: C₄₁H₇₂O₁₀SSi₅

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere; Molecular sieve;
DOI:10.1002/ejoc.201101267