phenyl 1-(4-chlorophenyl)-4-(3,4-dimethoxyphenyl)-2-naphthoate

Base Information

Chemical Name:phenyl 1-(4-chlorophenyl)-4-(3,4-dimethoxyphenyl)-2-naphthoate
CAS No.:1333383-01-9
Molecular Formula:C₃₁H₂₃ClO₄
Molecular Weight:494.974
Hs Code.:

Synonyms:phenyl 1-(4-chlorophenyl)-4-(3,4-dimethoxyphenyl)-2-naphthoate

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Chemical Property of phenyl 1-(4-chlorophenyl)-4-(3,4-dimethoxyphenyl)-2-naphthoate

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Technology Process of phenyl 1-(4-chlorophenyl)-4-(3,4-dimethoxyphenyl)-2-naphthoate

There total 2 articles about phenyl 1-(4-chlorophenyl)-4-(3,4-dimethoxyphenyl)-2-naphthoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1220707-81-2
phenyl 1,4-bis(trifluoromethylsulfonyloxy)-2-naphthoate

: 1679-18-1
4-Chlorophenylboronic acid

: 122775-35-3
3,4-Dimethoxyphenylboronic acid

: 1333383-01-9
phenyl 1-(4-chlorophenyl)-4-(3,4-dimethoxyphenyl)-2-naphthoate

Guidance literature:: phenyl 1,4-bis(trifluoromethylsulfonyloxy)-2-naphthoate; 4-Chlorophenylboronic acid; With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 95 ℃; for 7h; Inert atmosphere;

3,4-Dimethoxyphenylboronic acid; With potassium phosphate; In 1,4-dioxane; at 20 - 110 ℃; for 6h; Inert atmosphere;
DOI:10.1055/s-0030-1260054

Reference yield:

: 54978-55-1
phenyl 1,4-dihydroxynaphthalene-2-carboxylate

: 1333383-01-9
phenyl 1-(4-chlorophenyl)-4-(3,4-dimethoxyphenyl)-2-naphthoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 0.17 h / -78 °C / Inert atmosphere

1.2: 4 h / -78 - 0 °C / Inert atmosphere

2.1: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 7 h / 95 °C / Inert atmosphere

2.2: 6 h / 20 - 110 °C / Inert atmosphere

With pyridine; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; 2.1: Suzuki coupling / 2.2: Suzuki coupling;
DOI:10.1055/s-0030-1260054