C₂₁H₃₂N₂O₃

Base Information

Chemical Name:C₂₁H₃₂N₂O₃
CAS No.:1259040-27-1
Molecular Formula:C₂₁H₃₂N₂O₃
Molecular Weight:360.497
Hs Code.:

C<sub>21</sub>H<sub>32</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₁H₃₂N₂O₃

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Chemical Property of C₂₁H₃₂N₂O₃

Chemical Property:

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Technology Process of C₂₁H₃₂N₂O₃

There total 4 articles about C₂₁H₃₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₃₄N₂O₄

: 1259040-27-1
C₂₁H₃₂N₂O₃

Guidance literature:: With sodium tetrahydroborate; water; In ethanol; at 20 ℃; for 5h;

Reference yield:

: 146603-99-8
1-(1,1-dimethylethyl) 4-ethyl 4-(2-propenyl)-1,4-piperidinedicarboxylate

: 1259040-27-1
C₂₁H₃₂N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: ozone / methanol / 1 h / -78 °C

1.2: 15 h / 20 °C

2.1: acetic acid; sodium tris(acetoxy)borohydride / N,N-dimethyl-formamide / 21 h / 20 - 40 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / tetrahydrofuran / 2 h / -40 °C / Inert atmosphere

3.2: 0.5 h / -40 - 20 °C

4.1: lithium diisopropyl amide; N,N,N,N,N,N-hexamethylphosphoric triamide / n-heptane; tetrahydrofuran; ethylbenzene / 0.08 h / -78 °C / Inert atmosphere

4.2: 1.5 h

5.1: water; sodium tetrahydroborate / ethanol / 5 h / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; water; sodium tris(acetoxy)borohydride; diisobutylaluminium hydride; ozone; acetic acid; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; n-heptane; ethylbenzene; N,N-dimethyl-formamide;

Reference yield:

: 1228603-43-7
4-(2-oxoethyl)-piperidine-1,4-dicarboxylic acid 1-tert-butyl ester 4-ethyl ester

: 1259040-27-1
C₂₁H₃₂N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid; sodium tris(acetoxy)borohydride / N,N-dimethyl-formamide / 21 h / 20 - 40 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / tetrahydrofuran / 2 h / -40 °C / Inert atmosphere

2.2: 0.5 h / -40 - 20 °C

3.1: lithium diisopropyl amide; N,N,N,N,N,N-hexamethylphosphoric triamide / n-heptane; tetrahydrofuran; ethylbenzene / 0.08 h / -78 °C / Inert atmosphere

3.2: 1.5 h

4.1: water; sodium tetrahydroborate / ethanol / 5 h / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; water; sodium tris(acetoxy)borohydride; diisobutylaluminium hydride; acetic acid; lithium diisopropyl amide; In tetrahydrofuran; ethanol; n-heptane; ethylbenzene; N,N-dimethyl-formamide;