C₄₆H₇₀O₅S₂Si

Base Information

Chemical Name:C₄₆H₇₀O₅S₂Si
CAS No.:1380328-07-3
Molecular Formula:C₄₆H₇₀O₅S₂Si
Molecular Weight:795.276
Hs Code.:

C<sub>46</sub>H<sub>70</sub>O<sub>5</sub>S<sub>2</sub>Si

Synonyms:C₄₆H₇₀O₅S₂Si

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Chemical Property of C₄₆H₇₀O₅S₂Si

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Technology Process of C₄₆H₇₀O₅S₂Si

There total 6 articles about C₄₆H₇₀O₅S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1380328-06-2
C₁₆H₃₄OS₂Si

: 1380328-05-1
(R)-2-((2R,3R)-7-(3-(benzyloxy)phenyl)-3-((4-methoxybenzyl)oxy)heptan-2-yl)oxirane

: 1380328-07-3
C₄₆H₇₀O₅S₂Si

Guidance literature:: C₁₆H₃₄OS₂Si; With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 0.75h; Inert atmosphere;

(R)-2-((2R,3R)-7-(3-(benzyloxy)phenyl)-3-((4-methoxybenzyl)oxy)heptan-2-yl)oxirane; In tetrahydrofuran; hexane; at 4 ℃; for 18h; Inert atmosphere;
DOI:10.1021/jm300566h

Reference yield:

: 289034-17-9
C₁₈H₂₀O₂

: 1380328-07-3
C₄₆H₇₀O₅S₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium; potassium tert-butylate / tetrahydrofuran; hexane / 0.25 h / -40 °C / Inert atmosphere

1.2: 0.5 h / -78 °C / Inert atmosphere

1.3: 2 h / -78 °C / Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 4 °C

2.2: 0.25 h / 20 °C

3.1: iodine(I) bromide / dichloromethane; toluene / 2 h / -78 °C

3.2: 0.75 h / 20 °C

4.1: methanol; sodium methylate / 2 h / 20 - 50 °C

5.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 55 h / 20 °C

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / 20 °C / Inert atmosphere

6.2: 18 h / 4 °C / Inert atmosphere

With methanol; n-butyllithium; potassium tert-butylate; sodium methylate; sodium hexamethyldisilazane; iodine(I) bromide; sodium hydride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/jm300566h

Reference yield:

: C₂₇H₃₆O₄

: 1380328-07-3
C₄₆H₇₀O₅S₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: iodine(I) bromide / dichloromethane; toluene / 2 h / -78 °C

1.2: 0.75 h / 20 °C

2.1: methanol; sodium methylate / 2 h / 20 - 50 °C

3.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 55 h / 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / 20 °C / Inert atmosphere

4.2: 18 h / 4 °C / Inert atmosphere

With methanol; n-butyllithium; sodium methylate; iodine(I) bromide; sodium hydride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/jm300566h