4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-N-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)benzamide

Base Information

Chemical Name:4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-N-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)benzamide
CAS No.:1394389-42-4
Molecular Formula:C₂₆H₃₄BNO₃
Molecular Weight:419.372
Hs Code.:

Synonyms:4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-N-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)benzamide

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Chemical Property of 4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-N-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)benzamide

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Technology Process of 4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-N-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)benzamide

There total 2 articles about 4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-N-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1394389-41-3
4-bromo-N-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)benzamide

: 201733-56-4
2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-5,5-dimethyl-1,3,2-dioxaborinane

: 1394389-42-4
4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-N-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)benzamide

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; dimethyl sulfoxide; at 90 ℃; for 16h;
DOI:10.1021/ml300160w DOI:10.1021/ml300160w

Reference yield:

: 94497-51-5
Am80

: 1394389-42-4
4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-N-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / tetrahydrofuran / 20 °C / Inert atmosphere; Glovebox

2: C₄₂H₇₁FNiP₂ / tetrahydrofuran / 16 h / 115 °C / Inert atmosphere; Sealed tube

With C₄₂H₇₁FNiP₂; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; In tetrahydrofuran;
DOI:10.1021/jacs.9b08961

Reference yield:

: 67-56-1
methanol

: 1394389-42-4
4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-N-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)benzamide

: 10456-04-9
11C-carbon monooxide

: 1394389-39-9
C₂₂⁽¹¹⁾CH₂₇NO₃

Guidance literature:: With palladium diacetate; triphenylphosphine; p-benzoquinone; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h; Radiolysis; Inert atmosphere;
DOI:10.1021/ml300160w