Stearic acid 2β-phenyl-1,3-dioxan-5β-yl ester

Base Information

• Chemical Name: Stearic acid 2β-phenyl-1,3-dioxan-5β-yl ester
• CAS No.: 10588-88-2
• Molecular Formula: C₂₈H₄₆O₄
• Molecular Weight: 446.671
• Mol file: 10588-88-2.mol

Synonyms:cis-2-phenyl-5-stearoyloxy-[1,3]dioxane

Chemical Property of Stearic acid 2β-phenyl-1,3-dioxan-5β-yl ester

Chemical Property:

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Stearic acid 2β-phenyl-1,3-dioxan-5β-yl ester

There total 3 articles about Stearic acid 2β-phenyl-1,3-dioxan-5β-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

stearic acid (57-11-4) + 2-phenyl-[1,3]dioxan-5-ol (1708-40-3) → C28H46O4 (10564-35-9) + cis-2-phenyl-5-stearoyloxy-[1,3]dioxane (10588-88-2)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 72h; Inert atmosphere;

DOI:10.1016/j.tet.2010.09.070

Reference yield:

Stearoyl chloride (112-76-5) + cis-5-hydroxyl-2-phenyl-1,3-dioxane (1708-40-3,4141-19-9,4141-20-2) → cis-2-phenyl-5-stearoyloxy-[1,3]dioxane (10588-88-2)

Guidance literature:

With pyridine;

Reference yield:

benzaldehyde (100-52-7) + stearic acid (57-11-4) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → C28H46O4 (10564-35-9) + C28H46O4 (56599-43-0,56599-88-3) + C28H46O4 (56599-43-0,56599-88-3) + cis-2-phenyl-5-stearoyloxy-[1,3]dioxane (10588-88-2)

Guidance literature:

benzaldehyde; glycerol; Inert atmosphere;

stearic acid; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1016/j.tet.2010.09.070

upstream raw materials:

Stearoyl chloride

cis-5-hydroxyl-2-phenyl-1,3-dioxane

benzaldehyde

stearic acid

Downstream raw materials:

Methyl stearate

cis-5-hydroxyl-2-phenyl-1,3-dioxane

Refernces