phenyl 2,3-O-(2',3'-dimethoxy-2',3'-dimethylbutane)-1-thio-β-L-fucopyranoside

Base Information

Chemical Name:phenyl 2,3-O-(2',3'-dimethoxy-2',3'-dimethylbutane)-1-thio-β-L-fucopyranoside
CAS No.:912478-19-4
Molecular Formula:C₁₈H₂₆O₆S
Molecular Weight:370.467
Hs Code.:

Synonyms:phenyl 2,3-O-(2',3'-dimethoxy-2',3'-dimethylbutane)-1-thio-β-L-fucopyranoside

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Chemical Property of phenyl 2,3-O-(2',3'-dimethoxy-2',3'-dimethylbutane)-1-thio-β-L-fucopyranoside

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Technology Process of phenyl 2,3-O-(2',3'-dimethoxy-2',3'-dimethylbutane)-1-thio-β-L-fucopyranoside

There total 5 articles about phenyl 2,3-O-(2',3'-dimethoxy-2',3'-dimethylbutane)-1-thio-β-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 67-56-1
methanol

: 431-03-8
dimethylglyoxal

: 187233-24-5
phenyl 6-deoxy-1-thio-β-L-galactopyranoside

: 912478-19-4
phenyl 2,3-O-(2',3'-dimethoxy-2',3'-dimethylbutane)-1-thio-β-L-fucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; trimethyl orthoformate; for 16h; Heating;
DOI:10.1021/ja064619y

Reference yield: 70.0%

: 67-56-1
methanol

: 431-03-8
dimethylglyoxal

: 187233-24-5
phenyl 6-deoxy-1-thio-β-L-galactopyranoside

: 149-73-5
trimethyl orthoformate

: 912478-19-4
phenyl 2,3-O-(2',3'-dimethoxy-2',3'-dimethylbutane)-1-thio-β-L-fucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; for 15h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201403074

Reference yield:

: 6696-41-9
alpha-L-fucose

: 912478-19-4
phenyl 2,3-O-(2',3'-dimethoxy-2',3'-dimethylbutane)-1-thio-β-L-fucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 1 h / 100 °C

2: boron trifluoride diethyl etherate / dichloromethane / 14 h / 0 - 20 °C

3: methanol; sodium methylate / 3 h

4: camphor-10-sulfonic acid / 15 h / Inert atmosphere; Reflux

With pyridine; methanol; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; sodium methylate; In dichloromethane;
DOI:10.1002/ejoc.201403074