N-Benzyloxy-N-(5-tert-butoxycarbonylamino-pentyl)-succinamic acid methyl ester

Base Information

Chemical Name:N-Benzyloxy-N-(5-tert-butoxycarbonylamino-pentyl)-succinamic acid methyl ester
CAS No.:153492-10-5
Molecular Formula:C₂₂H₃₄N₂O₆
Molecular Weight:422.522
Hs Code.:

Synonyms:N-Benzyloxy-N-(5-tert-butoxycarbonylamino-pentyl)-succinamic acid methyl ester

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Chemical Property of N-Benzyloxy-N-(5-tert-butoxycarbonylamino-pentyl)-succinamic acid methyl ester

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Technology Process of N-Benzyloxy-N-(5-tert-butoxycarbonylamino-pentyl)-succinamic acid methyl ester

There total 5 articles about N-Benzyloxy-N-(5-tert-butoxycarbonylamino-pentyl)-succinamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 153492-09-2
1-<(tert-Butoxycarbonyl)amino>-5-<(benzyloxy)amino>pentane

: 1490-25-1
succinic acid monomethylester chloride

: 153492-10-5
N-Benzyloxy-N-(5-tert-butoxycarbonylamino-pentyl)-succinamic acid methyl ester

Guidance literature:: With pyridine; In acetonitrile; for 12h; Ambient temperature;
DOI:10.1021/jo00079a007

Reference yield:

: 90195-00-9
N-<(2,2,2-trichloroethoxy)carbonyl>-O-benzylhydroxylamine

: 153492-10-5
N-Benzyloxy-N-(5-tert-butoxycarbonylamino-pentyl)-succinamic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95.5 percent / Ph₃P, DEAD / tetrahydrofuran / 16 h / Ambient temperature

2: 94 percent / Zn, 1 M aq. KH₂PO₄ / tetrahydrofuran / 3 h / Ambient temperature

3: 97 percent / pyridine / acetonitrile / 12 h / Ambient temperature

With pyridine; potassium dihydrogenphosphate; triphenylphosphine; zinc; diethylazodicarboxylate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00079a007

Reference yield:

: 75178-90-4
N-(tert-butyloxycarbonyl)-5-aminopentanol

: 153492-10-5
N-Benzyloxy-N-(5-tert-butoxycarbonylamino-pentyl)-succinamic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95.5 percent / Ph₃P, DEAD / tetrahydrofuran / 16 h / Ambient temperature

2: 94 percent / Zn, 1 M aq. KH₂PO₄ / tetrahydrofuran / 3 h / Ambient temperature

3: 97 percent / pyridine / acetonitrile / 12 h / Ambient temperature

With pyridine; potassium dihydrogenphosphate; triphenylphosphine; zinc; diethylazodicarboxylate; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00079a007