1,2?bis(benzimidazol?1?yl)ethane

Base Information

Chemical Name:1,2?bis(benzimidazol?1?yl)ethane
CAS No.:49629-31-4
Molecular Formula:C₁₆H₁₄N₄
Molecular Weight:262.314
Hs Code.:

Synonyms:1,2?bis(benzimidazol?1?yl)ethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2?bis(benzimidazol?1?yl)ethane

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Technology Process of 1,2?bis(benzimidazol?1?yl)ethane

There total 2 articles about 1,2?bis(benzimidazol?1?yl)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 51-17-2,79351-71-6
benzoimidazole

: 106-93-4
ethylene dibromide

: 26972-40-7
1-vinylbenzimidazole

: 49629-31-4
1,2?bis(benzimidazol?1?yl)ethane

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide; In toluene; at 60 - 80 ℃; for 24h;

Reference yield: 55.0%

: 51-17-2,79351-71-6
benzoimidazole

: 107-06-2,52399-93-6
1,2-dichloro-ethane

: 26972-40-7
1-vinylbenzimidazole

: 49629-31-4
1,2?bis(benzimidazol?1?yl)ethane

Guidance literature:: With tetrabutylammomium bromide; potassium carbonate; at 60 ℃; for 48h;

Reference yield: 85.0%

: bis[4-(trimethylammonio)benzenethiolate]mercury(II)

: 49629-31-4
1,2?bis(benzimidazol?1?yl)ethane

: catena-poly[[(bis[4-(trimethylammonio)benzenethiolate-κS]mercury(II))-μ-1,1'-(ethane-1,2-diyl)-bis(1H-benzimidazole)-κ**(2)N**(3):N**(3')] bis(hexafluoridophosphate) 0.25-hydrate]

Guidance literature:: In methanol; acetonitrile; to soln. of Hg compd. in MeCN added soln. of benzimidazole deriv. in MeOH; mixt. stirred for 1 h; filtered; Et2O layered onto filtrate, left for several d; ppt. collectedby filtration, washed with Et2O, dried in vac.; elem. anal.;
DOI:10.1107/S0108270111021512