4-nitrophenylsulphur trifluoride

Base Information

• Chemical Name: 4-nitrophenylsulphur trifluoride
• CAS No.: 1526-28-9
• Molecular Formula: C₆H₄F₃NO₂S
• Molecular Weight: 211.164
• Mol file: 1526-28-9.mol

Synonyms:4-nitrophenylsulphur trifluoride

Chemical Property of 4-nitrophenylsulphur trifluoride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4-nitrophenylsulphur trifluoride

There total 3 articles about 4-nitrophenylsulphur trifluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

di(p-nitrophenyl) disulfide (100-32-3) → 4-nitrophenylsulphur trifluoride (1526-28-9)

Guidance literature:

With potassium fluoride; chlorine; In acetonitrile; at 20 ℃; for 4.5h;

DOI:10.1081/SCC-120021841

Reference yield:

di(p-nitrophenyl) disulfide (100-32-3) → 1-nitro-4-(pentafluorosulfanyl)benzene (2613-27-6) + 4-nitrophenylsulphur trifluoride (1526-28-9)

Guidance literature:

With fluorine; In acetonitrile; at -35 - -25 ℃;

Reference yield:

4-nitrobenzenesulfenyl chloride (937-32-6) → 4-nitrophenylsulphur trifluoride (1526-28-9)

Guidance literature:

With fluorine; cesium fluoride; In acetonitrile; at -35 - -25 ℃;

upstream raw materials:

di(p-nitrophenyl) disulfide

4-nitrobenzenesulfenyl chloride

Downstream raw materials:

1-nitro-4-(pentafluorosulfanyl)benzene

2-fluoroethyl p-nitrophenylsulfinate