(6-(2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzylthio)nicotinic)pivalic anhydride

Base Information

Chemical Name:(6-(2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzylthio)nicotinic)pivalic anhydride
CAS No.:1312301-83-9
Molecular Formula:C₂₃H₂₈BNO₅S
Molecular Weight:441.356
Hs Code.:

Synonyms:(6-(2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzylthio)nicotinic)pivalic anhydride

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Chemical Property of (6-(2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzylthio)nicotinic)pivalic anhydride

Chemical Property:

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Technology Process of (6-(2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzylthio)nicotinic)pivalic anhydride

There total 5 articles about (6-(2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzylthio)nicotinic)pivalic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₀BNO₄S

: 3282-30-2
pivaloyl chloride

: 1312301-83-9
(6-(2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzylthio)nicotinic)pivalic anhydride

Guidance literature:: With triethylamine; In toluene; at 20 ℃; Cooling with ice; Inert atmosphere;

Reference yield:

: 1240496-03-0
6-(2-boronobenzylthio)nicotinic acid

: 3282-30-2
pivaloyl chloride

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 1312301-83-9
(6-(2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzylthio)nicotinic)pivalic anhydride

Guidance literature:: 6-(2-boronobenzylthio)nicotinic acid; 2,2-Dimethyl-1,3-propanediol; In toluene; for 24h; Reflux; Inert atmosphere;

pivaloyl chloride; With triethylamine; In toluene; at 20 ℃; for 2h;

Reference yield:

: 17624-07-6,92823-43-3
6-Mercapto-nicotinic acid

: 1312301-83-9
(6-(2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzylthio)nicotinic)pivalic anhydride

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / N,N-dimethyl-formamide / 1 h / 60 °C

2: toluene / 24 h / Reflux

3: triethylamine / toluene / 2 h / 0 - 20 °C / Inert atmosphere

With triethylamine; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm500827t