1-(4-chloro-phenyl)-2-[(Z)-(4-dimethylamino-phenyl)-oxy-imino]-ethanone

Base Information

• Chemical Name: 1-(4-chloro-phenyl)-2-[(Z)-(4-dimethylamino-phenyl)-oxy-imino]-ethanone
• CAS No.: 52626-24-1
• Molecular Formula: C₁₆H₁₅ClN₂O₂
• Molecular Weight: 302.76
• Mol file: 52626-24-1.mol

Synonyms:1-(4-chloro-phenyl)-2-[(Z)-(4-dimethylamino-phenyl)-oxy-imino]-ethanone

Chemical Property of 1-(4-chloro-phenyl)-2-[(Z)-(4-dimethylamino-phenyl)-oxy-imino]-ethanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(4-chloro-phenyl)-2-[(Z)-(4-dimethylamino-phenyl)-oxy-imino]-ethanone

There total 1 articles about 1-(4-chloro-phenyl)-2-[(Z)-(4-dimethylamino-phenyl)-oxy-imino]-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2-(4-chlorophenyl)-2-oxoethyl)pyridinium bromide (26031-66-3) + p-dimethylaminonitrosobenzene (138-89-6) → 1-(4-chloro-phenyl)-2-[(Z)-(4-dimethylamino-phenyl)-oxy-imino]-ethanone (52626-24-1)

Guidance literature:

With sodium hydroxide; ethanol;

Reference yield:

1-(4-chloro-phenyl)-2-[(Z)-(4-dimethylamino-phenyl)-oxy-imino]-ethanone (52626-24-1) → para-chlorobenzoic acid (74-11-3)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous ethanol

2: ethanol; diethyl ether; aqueous NaOH-solution

With sodium hydroxide; diethyl ether; ethanol;

Reference yield:

1-(4-chloro-phenyl)-2-[(Z)-(4-dimethylamino-phenyl)-oxy-imino]-ethanone (52626-24-1) → [7-(4-chloro-phenyl)-1-(4-dimethylamino-phenyl)-4-phenyl-(3ar,7ac)-1,3,3a,7a-tetrahydro-isoxazolo[3,4-d]pyridazin-3c-yl]-phenyl-methanone (52626-27-4)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / Ambient temperature

2: NH₂NH₂ / ethanol / 0.25 h / Heating

With hydrazine; In ethanol; benzene;

DOI:10.1139/v74-126

upstream raw materials:

1-(2-(4-chlorophenyl)-2-oxoethyl)pyridinium bromide

p-dimethylaminonitrosobenzene

Downstream raw materials:

1-(4-Dimethylaminophenylimino-)-2-keto-2-(4-chlorphenyl-)-propionitril

C-(4-chloro-phenyl)-C',C''-diphenyl-C,C',C''-[2-(4-dimethylamino-phenyl)-isoxazolidine-3r,4c,5t-triyl]-tris-methanone

4-chlorophenylglyoxylic acid

3-(4-chloro-phenyl)-2,3-dioxo-propionic acid amide