3-(p-azidophenyl)-2-oxopropanal

Base Information

Chemical Name:3-(p-azidophenyl)-2-oxopropanal
CAS No.:264608-82-4
Molecular Formula:C₉H₇N₃O₂
Molecular Weight:189.173
Hs Code.:

Synonyms:3-(p-azidophenyl)-2-oxopropanal

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Chemical Property of 3-(p-azidophenyl)-2-oxopropanal

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Technology Process of 3-(p-azidophenyl)-2-oxopropanal

There total 5 articles about 3-(p-azidophenyl)-2-oxopropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 264608-81-3
3-(p-azidophenyl)-2-oxopropyl nitrate

: 264608-82-4
3-(p-azidophenyl)-2-oxopropanal

Guidance literature:: With sodium acetate; In dimethyl sulfoxide; at 20 ℃; for 1h;
DOI:10.1246/bcsj.73.465

Reference yield:

: 62893-37-2
2-(4-azidophenyl)acetic acid

: 264608-82-4
3-(p-azidophenyl)-2-oxopropanal

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / benzene / 18 h / 20 °C

2: 5.0 g / diethyl ether / 1 h / 0 °C

3: 90 percent / HBr / diethyl ether / 0.33 h / 0 °C

4: 86 percent / AgNO₃ / acetonitrile / 28 h / 20 °C

5: 100 percent / sodium acetate trihydrate / dimethylsulfoxide / 1 h / 20 °C

With thionyl chloride; hydrogen bromide; sodium acetate; silver nitrate; In diethyl ether; dimethyl sulfoxide; acetonitrile; benzene; 1: Substitution / 2: Acylation / 3: Substitution / 4: Substitution / 5: Oxidation;
DOI:10.1246/bcsj.73.465

Reference yield:

: 247150-03-4
2-(4-azidophenyl)acetyl chloride

: 264608-82-4
3-(p-azidophenyl)-2-oxopropanal

Guidance literature:: Multi-step reaction with 4 steps

1: 5.0 g / diethyl ether / 1 h / 0 °C

2: 90 percent / HBr / diethyl ether / 0.33 h / 0 °C

3: 86 percent / AgNO₃ / acetonitrile / 28 h / 20 °C

4: 100 percent / sodium acetate trihydrate / dimethylsulfoxide / 1 h / 20 °C

With hydrogen bromide; sodium acetate; silver nitrate; In diethyl ether; dimethyl sulfoxide; acetonitrile; 1: Acylation / 2: Substitution / 3: Substitution / 4: Oxidation;
DOI:10.1246/bcsj.73.465