3-(p-azidophenyl)-2-oxopropyl nitrate

Base Information

Chemical Name:3-(p-azidophenyl)-2-oxopropyl nitrate
CAS No.:264608-81-3
Molecular Formula:C₉H₈N₄O₄
Molecular Weight:236.187
Hs Code.:

Synonyms:3-(p-azidophenyl)-2-oxopropyl nitrate

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Chemical Property of 3-(p-azidophenyl)-2-oxopropyl nitrate

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Technology Process of 3-(p-azidophenyl)-2-oxopropyl nitrate

There total 4 articles about 3-(p-azidophenyl)-2-oxopropyl nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 264608-80-2
1-(p-azidophenyl)-3-bromo-2-propanone

: 264608-81-3
3-(p-azidophenyl)-2-oxopropyl nitrate

Guidance literature:: With silver nitrate; In acetonitrile; at 20 ℃; for 28h;
DOI:10.1246/bcsj.73.465

Reference yield:

: 62893-37-2
2-(4-azidophenyl)acetic acid

: 264608-81-3
3-(p-azidophenyl)-2-oxopropyl nitrate

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / benzene / 18 h / 20 °C

2: 5.0 g / diethyl ether / 1 h / 0 °C

3: 90 percent / HBr / diethyl ether / 0.33 h / 0 °C

4: 86 percent / AgNO₃ / acetonitrile / 28 h / 20 °C

With thionyl chloride; hydrogen bromide; silver nitrate; In diethyl ether; acetonitrile; benzene; 1: Substitution / 2: Acylation / 3: Substitution / 4: Substitution;
DOI:10.1246/bcsj.73.465

Reference yield:

: 247150-03-4
2-(4-azidophenyl)acetyl chloride

: 264608-81-3
3-(p-azidophenyl)-2-oxopropyl nitrate

Guidance literature:: Multi-step reaction with 3 steps

1: 5.0 g / diethyl ether / 1 h / 0 °C

2: 90 percent / HBr / diethyl ether / 0.33 h / 0 °C

3: 86 percent / AgNO₃ / acetonitrile / 28 h / 20 °C

With hydrogen bromide; silver nitrate; In diethyl ether; acetonitrile; 1: Acylation / 2: Substitution / 3: Substitution;
DOI:10.1246/bcsj.73.465