ethyl 2-{1-carbamoyl-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinyl}ethanoate

Base Information

Chemical Name:ethyl 2-{1-carbamoyl-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinyl}ethanoate
CAS No.:55227-60-6
Molecular Formula:C₁₆H₁₆N₄O₆
Molecular Weight:360.326
Hs Code.:

Synonyms:ethyl 2-{1-carbamoyl-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinyl}ethanoate

Suppliers and Price of ethyl 2-{1-carbamoyl-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinyl}ethanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-[1-(Aminocarbonyl)-2-[[5-(4-nitrophenyl)-2-furanyl]methylene]hydrazinyl]-aceticAcidEthylEster
5mg
$ 55.00

Total 4 raw suppliers

Chemical Property of ethyl 2-{1-carbamoyl-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinyl}ethanoate

Chemical Property:

Purity/Quality:

> 95% ^*data from raw suppliers

2-[1-(Aminocarbonyl)-2-[[5-(4-nitrophenyl)-2-furanyl]methylene]hydrazinyl]-aceticAcidEthylEster ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 2-[1-(Aminocarbonyl)-2-[[5-(4-nitrophenyl)-2-furanyl]methylene]hydrazinyl]-acetic Acid Ethyl Ester is an intermediate used in the synthesis of 1-(5-Phenylfurfurylideneamino)hydantoins.

Technology Process of ethyl 2-{1-carbamoyl-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinyl}ethanoate

There total 3 articles about ethyl 2-{1-carbamoyl-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinyl}ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.2%

: 1357016-88-6
4-nitrophenyl 1-(2-ethoxy-2-oxoethyl)-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinecarboxylate

: 55227-60-6
ethyl 2-{1-carbamoyl-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinyl}ethanoate

Guidance literature:: With ammonia; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1016/j.bmc.2011.10.077

Reference yield:

: 76834-61-2
ethyl 2-{2-[5-(4-nitrophenyl)furfurylidene]hydrazino}acetate

: 55227-60-6
ethyl 2-{1-carbamoyl-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinyl}ethanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 12 h / 0 - 20 °C

2: ammonia / N,N-dimethyl-formamide / 12 h / 20 °C

With ammonia; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.10.077

Reference yield:

: 7147-77-5
5-(4-nitrophenyl)-2-furaldehyde

: 55227-60-6
ethyl 2-{1-carbamoyl-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinyl}ethanoate

Guidance literature:: Multi-step reaction with 3 steps

1: water; N,N-dimethyl-formamide / 24 h / 20 °C

2: triethylamine / dichloromethane / 12 h / 0 - 20 °C

3: ammonia / N,N-dimethyl-formamide / 12 h / 20 °C

With ammonia; triethylamine; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.10.077