4-nitrophenyl 1-(2-ethoxy-2-oxoethyl)-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinecarboxylate

Base Information

• Chemical Name: 4-nitrophenyl 1-(2-ethoxy-2-oxoethyl)-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinecarboxylate
• CAS No.: 1357016-88-6
• Molecular Formula: C₂₂H₁₈N₄O₉
• Molecular Weight: 482.406

Synonyms:4-nitrophenyl 1-(2-ethoxy-2-oxoethyl)-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinecarboxylate

Chemical Property of 4-nitrophenyl 1-(2-ethoxy-2-oxoethyl)-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-nitrophenyl 1-(2-ethoxy-2-oxoethyl)-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinecarboxylate

There total 2 articles about 4-nitrophenyl 1-(2-ethoxy-2-oxoethyl)-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

ethyl 2-{2-[5-(4-nitrophenyl)furfurylidene]hydrazino}acetate (76834-61-2) + 4-Nitrophenyl chloroformate (7693-46-1) → 4-nitrophenyl 1-(2-ethoxy-2-oxoethyl)-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinecarboxylate (1357016-88-6)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 12h;

DOI:10.1016/j.bmc.2011.10.077

Reference yield:

5-(4-nitrophenyl)-2-furaldehyde (7147-77-5) → 4-nitrophenyl 1-(2-ethoxy-2-oxoethyl)-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinecarboxylate (1357016-88-6)

Guidance literature:

Multi-step reaction with 2 steps

1: water; N,N-dimethyl-formamide / 24 h / 20 °C

2: triethylamine / dichloromethane / 12 h / 0 - 20 °C

With triethylamine; In dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2011.10.077

Reference yield: 65.2%

4-nitrophenyl 1-(2-ethoxy-2-oxoethyl)-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinecarboxylate (1357016-88-6) → ethyl 2-{1-carbamoyl-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinyl}ethanoate (55227-60-6)

Guidance literature:

With ammonia; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

DOI:10.1016/j.bmc.2011.10.077

upstream raw materials:

ethyl 2-{2-[5-(4-nitrophenyl)furfurylidene]hydrazino}acetate

4-Nitrophenyl chloroformate

5-(4-nitrophenyl)-2-furaldehyde

Downstream raw materials:

C₁₄H₁₀N₃⁽¹³⁾NO₅

ethyl 2-{1-carbamoyl-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinyl}ethanoate

C₁₆H₁₆N₃⁽¹³⁾NO₆

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1357016-88-6 4-nitrophenyl 1-(2-ethoxy-2-oxoethyl)-2-[(5-(4-nitrophenyl)furan-2-yl)methylene]hydrazinecarboxylate

Send

Send

Metric Ton KG G Pound L ML

Send

Send