(3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene-1,1-diyl)dibenzene

Base Information

• Chemical Name: (3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene-1,1-diyl)dibenzene
• CAS No.: 1539-96-4
• Molecular Formula: C₁₆H₁₀F₆
• Molecular Weight: 316.246
• Mol file: 1539-96-4.mol

Synonyms:(3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene-1,1-diyl)dibenzene

Chemical Property of (3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene-1,1-diyl)dibenzene

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of (3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene-1,1-diyl)dibenzene

There total 8 articles about (3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene-1,1-diyl)dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

1-(1-fluoro-2,2-diphenylvinyl)-1H-imidazole (72837-38-8) + (trifluoromethyl)trimethylsilane (81290-20-2) → (3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene-1,1-diyl)dibenzene (1539-96-4) + 1-(3,3,3-trifluoro-1,1-diphenylprop-1-en-2-yl)-1H-imidazole

Guidance literature:

With (bis(tricyclohexyl)phosphine)palladium(II) dichloride; tetrabutyl ammonium fluoride; In tetrahydrofuran; at 30 ℃; Reagent/catalyst; Temperature; Inert atmosphere;

DOI:10.1016/j.tet.2015.08.016

Reference yield: 31.0%

1,1-difluoro-2,2-diphenylethylene (569-72-2) + (trifluoromethyl)trimethylsilane (81290-20-2) → (3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene-1,1-diyl)dibenzene (1539-96-4)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 30 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2015.08.016

Reference yield:

1-(1-fluoro-2,2-diphenylvinyl)-1H-imidazole (72837-38-8) + (trifluoromethyl)trimethylsilane (81290-20-2) → (3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene-1,1-diyl)dibenzene (1539-96-4)

Guidance literature:

With dibromo[1,2-bis(diphenylphosphino)ethane]nickel(II); tetrabutyl ammonium fluoride; In tetrahydrofuran; at 60 ℃; Reagent/catalyst; Temperature; Inert atmosphere;

DOI:10.1016/j.tet.2015.08.016

upstream raw materials:

2,2-diphenyl-3,3-bis-trifluoromethyl-oxirane

2,2-bis(trifluoromethyl)-3,3-bisphenylthiirane

1,1-Diphenylethylene

1,1-difluoro-2,2-diphenylethylene