Benzyl 6α-Succinimidooxy-6β-(2,2,2-trichloroethoxycarbonylamino)penicillanate

Base Information

• Chemical Name: Benzyl 6α-Succinimidooxy-6β-(2,2,2-trichloroethoxycarbonylamino)penicillanate
• CAS No.: 104702-16-1
• Molecular Formula: C₂₂H₂₂Cl₃N₃O₈S
• Molecular Weight: 594.857

Synonyms:Benzyl 6α-Succinimidooxy-6β-(2,2,2-trichloroethoxycarbonylamino)penicillanate

Chemical Property of Benzyl 6α-Succinimidooxy-6β-(2,2,2-trichloroethoxycarbonylamino)penicillanate

Chemical Property:

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Technology Process of Benzyl 6α-Succinimidooxy-6β-(2,2,2-trichloroethoxycarbonylamino)penicillanate

There total 1 articles about Benzyl 6α-Succinimidooxy-6β-(2,2,2-trichloroethoxycarbonylamino)penicillanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

1-hydroxy-pyrrolidine-2,5-dione (6066-82-6) + benzyl 6β-(2,2,2-trichloroethoxycarbonylamino)-6α-(methylthio)penicillanate (86062-23-9) → Benzyl 6α-Succinimidooxy-6β-(2,2,2-trichloroethoxycarbonylamino)penicillanate (104702-16-1)

Guidance literature:

silver(I) acetate; In N,N-dimethyl-formamide;

DOI:10.1039/c39860000401

Reference yield: 54.0%

phenylmagnesium chloride (100-59-4) + Benzyl 6α-Succinimidooxy-6β-(2,2,2-trichloroethoxycarbonylamino)penicillanate (104702-16-1) → Benzyl 6α-Phenyl-6β-(2,2,2-trichloroethoxycarbonylamino)penicillanate (104702-17-2)

Guidance literature:

DOI:10.1039/c39860000401

Reference yield: 34.0%

phenylmagnesium chloride + Benzyl 6α-Succinimidooxy-6β-(2,2,2-trichloroethoxycarbonylamino)penicillanate (104702-16-1) → Benzyl 6α-Phenyl-6β-(2,2,2-trichloroethoxycarbonylamino)penicillanate (104702-17-2)

Guidance literature:

In tetrahydrofuran; diethyl ether; at -70 ℃;

upstream raw materials:

1-hydroxy-pyrrolidine-2,5-dione

benzyl 6β-(2,2,2-trichloroethoxycarbonylamino)-6α-(methylthio)penicillanate

Downstream raw materials:

Benzyl 6α-Phenyl-6β-(2,2,2-trichloroethoxycarbonylamino)penicillanate

Benzyl 6α-Amino-6β-phenylaminopenicillanate

Benzyl 6β-<(2R)-2-(4-Ethyl-2,3-dioxopiperazin-1-ylcarbonylamino)-2-phenylacetamido>-6α-phenylpenicillanate

Sodium 6β-<(2R)-2-(4-Ethyl-2,3-dioxopiperazin-1-ylcarbonylamino)-2-phenylacetamido>-6α-phenylpenicillanate

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