1-Ethenyl-2-(2-methoxypropan-2-yl)benzene

Base Information

Chemical Name:1-Ethenyl-2-(2-methoxypropan-2-yl)benzene
CAS No.:853270-96-9
Molecular Formula:C₁₂H₁₆O
Molecular Weight:176.258
Hs Code.:
DSSTox Substance ID:DTXSID101255708
Nikkaji Number:J2.192.062B

Synonyms:853270-96-9;DTXSID101255708;1-Ethenyl-2-(1-methoxy-1-methylethyl)benzene

Suppliers and Price of 1-Ethenyl-2-(2-methoxypropan-2-yl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Ethenyl-2-(2-methoxypropan-2-yl)benzene

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:176.120115130
Heavy Atom Count:13
Complexity:172

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C1=CC=CC=C1C=C)OC

Technology Process of 1-Ethenyl-2-(2-methoxypropan-2-yl)benzene

There total 2 articles about 1-Ethenyl-2-(2-methoxypropan-2-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 853271-14-4
2-(2-vinylphenyl)-2-propanol

: 74-88-4
methyl iodide

: 853270-96-9
1-[1-methoxy-1-methylethyl]-2-vinylbenzene

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jo0502293

Reference yield:

: 2039-88-5
2-bromostyrene

: 853270-96-9
1-[1-methoxy-1-methylethyl]-2-vinylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg / tetrahydrofuran / 2 h / 0 - 20 °C

1.2: 58 percent / tetrahydrofuran / 5 h / 0 °C

2.1: 95 percent / NaH / tetrahydrofuran / 20 °C

With sodium hydride; magnesium; In tetrahydrofuran;
DOI:10.1021/jo0502293

Reference yield: 81.0%

: 853270-96-9
1-[1-methoxy-1-methylethyl]-2-vinylbenzene

: 405-99-2
para-fluorostyrene

: 3-(4-fluorophenyl)-1,1,4-trimethyl-1,2,3,4-tetrahydronaphthalene

: 2,8-dimethoxy-6,6,12,12-tetramethyl-4b,5,6,10b,11,12-hexahydrochrysene

Guidance literature:: 1-[1-methoxy-1-methylethyl]-2-vinylbenzene; para-fluorostyrene; With n-butyllithium; (cyclopentadienyl)2ZrCl₂*but-1-ene; In tetrahydrofuran; hexane; at 20 ℃; for 3h;

With hydrogenchloride; In tetrahydrofuran; hexane;
DOI:10.1021/jo0502293