(1R,3S,3aR,6aS)-2-(2-Chloro-acetyl)-5-ethyl-3-(4-methoxy-phenyl)-1-methyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

Base Information

Chemical Name:(1R,3S,3aR,6aS)-2-(2-Chloro-acetyl)-5-ethyl-3-(4-methoxy-phenyl)-1-methyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester
CAS No.:898263-08-6
Molecular Formula:C₃₀H₂₆ClF₁₇N₂O₆
Molecular Weight:868.972
Hs Code.:

(1R,3S,3aR,6aS)-2-(2-Chloro-acetyl)-5-ethyl-3-(4-methoxy-phenyl)-1-methyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

Synonyms:(1R,3S,3aR,6aS)-2-(2-Chloro-acetyl)-5-ethyl-3-(4-methoxy-phenyl)-1-methyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

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Chemical Property of (1R,3S,3aR,6aS)-2-(2-Chloro-acetyl)-5-ethyl-3-(4-methoxy-phenyl)-1-methyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

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Technology Process of (1R,3S,3aR,6aS)-2-(2-Chloro-acetyl)-5-ethyl-3-(4-methoxy-phenyl)-1-methyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

There total 4 articles about (1R,3S,3aR,6aS)-2-(2-Chloro-acetyl)-5-ethyl-3-(4-methoxy-phenyl)-1-methyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 898262-98-1
(1R,3S,3aR,6aS)-5-Ethyl-3-(4-methoxy-phenyl)-1-methyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

: 79-04-9
chloroacetyl chloride

: 898263-08-6
(1R,3S,3aR,6aS)-2-(2-Chloro-acetyl)-5-ethyl-3-(4-methoxy-phenyl)-1-methyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 0.5h;
DOI:10.1002/ejoc.200600077

Reference yield:

: (S)-2-Amino-propionic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

: 898263-08-6
(1R,3S,3aR,6aS)-2-(2-Chloro-acetyl)-5-ethyl-3-(4-methoxy-phenyl)-1-methyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Et₃N / dimethylformamide / 0.33 h / 130 °C / microwave irradiation

2: 95 percent / Et₃N / CH₂Cl₂ / 0.5 h / 25 °C

With triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200600077

Reference yield:

: 128-53-0
N-Ethylmaleimide

: 898263-08-6
(1R,3S,3aR,6aS)-2-(2-Chloro-acetyl)-5-ethyl-3-(4-methoxy-phenyl)-1-methyl-4,6-dioxo-octahydro-pyrrolo[3,4-c]pyrrole-1-carboxylic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Et₃N / dimethylformamide / 0.33 h / 130 °C / microwave irradiation

2: 95 percent / Et₃N / CH₂Cl₂ / 0.5 h / 25 °C

With triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200600077