diethanolamine (S)-1-phenylethane-1-boronate

Base Information

Chemical Name:diethanolamine (S)-1-phenylethane-1-boronate
CAS No.:76101-96-7
Molecular Formula:C₁₂H₁₈BNO₂
Molecular Weight:219.091
Hs Code.:

Synonyms:diethanolamine (S)-1-phenylethane-1-boronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethanolamine (S)-1-phenylethane-1-boronate

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Technology Process of diethanolamine (S)-1-phenylethane-1-boronate

There total 1 articles about diethanolamine (S)-1-phenylethane-1-boronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 76110-80-0
(+)-pinanediol (S)-1-phenylethane-1-boronate

: 10294-34-5
boron trichloride

: 111-42-2
2,2'-iminobis[ethanol]

: 76101-96-7
diethanolamine (S)-1-phenylethane-1-boronate

Guidance literature:: In dichloromethane; boronic ester in CH2Cl2 added to BCl3 at -78°C, kept at 25°C for 2 h, concd., aq. work up, treated with diethanolamine in ether/isopropanol; recrystd. (CHCl3/C6H6); elem. anal.;
DOI:10.1021/ja00545a046

Reference yield: 79.0%

: 76101-96-7
diethanolamine (S)-1-phenylethane-1-boronate

: 22422-34-0
(1R,2R,3S,5R)-2,3-pinane diol

: 76155-63-0
(-)-pinandiol (S)-1-phenylethane-1-boronate

Guidance literature:: With hydrogenchloride; In diethyl ether; a suspn. of boronate ester was stirred under Ar with aq. HCl, ether soln. obtained was treated with diol for 4 h; distn., chromy. (silica, 10% ether in petroleum ether); elem. anal.;