5-Hydroxy-4-methoxy-3-<4-(methoxycarbonyl)phenoxy>benzoesaeure-methylester

Base Information

Chemical Name:5-Hydroxy-4-methoxy-3-<4-(methoxycarbonyl)phenoxy>benzoesaeure-methylester
CAS No.:118799-06-7
Molecular Formula:C₁₇H₁₆O₇
Molecular Weight:332.31
Hs Code.:

Synonyms:5-Hydroxy-4-methoxy-3-<4-(methoxycarbonyl)phenoxy>benzoesaeure-methylester

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Chemical Property of 5-Hydroxy-4-methoxy-3-<4-(methoxycarbonyl)phenoxy>benzoesaeure-methylester

Chemical Property:

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Technology Process of 5-Hydroxy-4-methoxy-3-<4-(methoxycarbonyl)phenoxy>benzoesaeure-methylester

There total 1 articles about 5-Hydroxy-4-methoxy-3-<4-(methoxycarbonyl)phenoxy>benzoesaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 619-42-1
4-methoxycarbonylphenyl bromide

: 24093-81-0
methyl 3,5-dihydroxy-4-methoxybenzoate

: 57466-23-6
4-Methoxy-3,5-bis<4-(methoxycarbonyl)phenoxy>benzoesaeure-methylester

: 118799-06-7
5-Hydroxy-4-methoxy-3-<4-(methoxycarbonyl)phenoxy>benzoesaeure-methylester

Guidance literature:: With potassium carbonate; copper(II) oxide; In pyridine; at 120 ℃; for 48h;

Reference yield:

: 118799-06-7
5-Hydroxy-4-methoxy-3-<4-(methoxycarbonyl)phenoxy>benzoesaeure-methylester

: 104290-38-2
perrottetin G

Guidance literature:: Multi-step reaction with 6 steps

1: 76 percent / K₂CO₃ / acetone / 5 h / Heating

2: 91 percent / LiAlH₄ / tetrahydrofuran

3: 80 percent / PBr₃ / CH₂Cl₂ / 3 h / Ambient temperature

4: 93 percent / acetonitrile / 1 h / Heating

5: 1N NaOCH₃, / CH₂Cl₂ / 1 h

6: 77 percent / H₂ / Pd/C / acetic acid

With lithium aluminium tetrahydride; hydrogen; sodium methylate; phosphorus tribromide; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetic acid; acetone; acetonitrile;

Reference yield:

: 118799-06-7
5-Hydroxy-4-methoxy-3-<4-(methoxycarbonyl)phenoxy>benzoesaeure-methylester

: 118799-12-5
Perrottetin G triacetat

Guidance literature:: Multi-step reaction with 7 steps

1: 76 percent / K₂CO₃ / acetone / 5 h / Heating

2: 91 percent / LiAlH₄ / tetrahydrofuran

3: 80 percent / PBr₃ / CH₂Cl₂ / 3 h / Ambient temperature

4: 93 percent / acetonitrile / 1 h / Heating

5: 1N NaOCH₃, / CH₂Cl₂ / 1 h

6: 77 percent / H₂ / Pd/C / acetic acid

7: 88 percent / pyridine / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; sodium methylate; phosphorus tribromide; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; pyridine; dichloromethane; acetic acid; acetone; acetonitrile;