2'-deoxy-2'-(3,5-diacetoxybenzamido)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)adenosine

Base Information

Chemical Name:2'-deoxy-2'-(3,5-diacetoxybenzamido)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)adenosine
CAS No.:218923-60-5
Molecular Formula:C₃₃H₄₈N₆O₉Si₂
Molecular Weight:728.95
Hs Code.:

Synonyms:2'-deoxy-2'-(3,5-diacetoxybenzamido)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)adenosine

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Chemical Property of 2'-deoxy-2'-(3,5-diacetoxybenzamido)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)adenosine

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Technology Process of 2'-deoxy-2'-(3,5-diacetoxybenzamido)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)adenosine

There total 2 articles about 2'-deoxy-2'-(3,5-diacetoxybenzamido)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 39192-49-9
3,5-diacetoxybenzoyl chloride

: 160056-49-5
2'-amino-2'-deoxy-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-adenosine

: 218923-60-5
2'-deoxy-2'-(3,5-diacetoxybenzamido)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)adenosine

Guidance literature:: With pyridine; In dichloromethane; for 3h; Heating;
DOI:10.1021/jm9802620

Reference yield:

: 35354-29-1
3,5-diacetoxybenzoic acid

: 218923-60-5
2'-deoxy-2'-(3,5-diacetoxybenzamido)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)adenosine

Guidance literature:: Multi-step reaction with 3 steps

1: PCl₅ / CH₂Cl₂ / 5 h / Ambient temperature

2: 60 percent / pyridine / CH₂Cl₂ / 3 h / Heating

3: 10 percent NH₃/MeOH / 0.25 h

With pyridine; methanol; phosphorus pentachloride; ammonia; In dichloromethane;
DOI:10.1021/jm9802620

Reference yield:

: 218923-60-5
2'-deoxy-2'-(3,5-diacetoxybenzamido)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)adenosine

: 2'-deoxy-2'-(3,5-dihydroxybenzamido)adenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 10 percent NH₃/MeOH / 0.25 h

2: NH₄F / methanol

With methanol; ammonium fluoride; ammonia; In methanol;
DOI:10.1021/jm9802620