2-{3-[(2,6-dioxocyclohexyl)carbonyl]-6-(methylsulfonyl)-2-(trifluoromethyl)phenoxy}-N,N-diethylacetamide

Base Information

Chemical Name:2-{3-[(2,6-dioxocyclohexyl)carbonyl]-6-(methylsulfonyl)-2-(trifluoromethyl)phenoxy}-N,N-diethylacetamide
CAS No.:1329602-24-5
Molecular Formula:C₂₁H₂₄F₃NO₇S
Molecular Weight:491.485
Hs Code.:

Synonyms:2-{3-[(2,6-dioxocyclohexyl)carbonyl]-6-(methylsulfonyl)-2-(trifluoromethyl)phenoxy}-N,N-diethylacetamide

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Chemical Property of 2-{3-[(2,6-dioxocyclohexyl)carbonyl]-6-(methylsulfonyl)-2-(trifluoromethyl)phenoxy}-N,N-diethylacetamide

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Technology Process of 2-{3-[(2,6-dioxocyclohexyl)carbonyl]-6-(methylsulfonyl)-2-(trifluoromethyl)phenoxy}-N,N-diethylacetamide

There total 5 articles about 2-{3-[(2,6-dioxocyclohexyl)carbonyl]-6-(methylsulfonyl)-2-(trifluoromethyl)phenoxy}-N,N-diethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 39096-01-0
N,N-diethyl-2-hydroxyacetamide

: 1329602-25-6
2-[3-fluoro-4-(methylsulfonyl)-2-(trifluoromethyl)benzoyl]cyclo-hexane-1,3-dione

: 1329602-24-5
2-{3-[(2,6-dioxocyclohexyl)carbonyl]-6-(methylsulfonyl)-2-(trifluoromethyl)phenoxy}-N,N-diethylacetamide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃;

Reference yield:

: 53056-21-6
2-(benzyloxy)-N,N-diethylacetamide

: 1329602-24-5
2-{3-[(2,6-dioxocyclohexyl)carbonyl]-6-(methylsulfonyl)-2-(trifluoromethyl)phenoxy}-N,N-diethylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 24 h

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 °C

With hydrogen; sodium hydride; palladium 10% on activated carbon; In ethyl acetate; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 159329-01-8
3-fluoro-4-(methylsulphenyl)-2-trifluoromethylbenzoic acid

: 1329602-24-5
2-{3-[(2,6-dioxocyclohexyl)carbonyl]-6-(methylsulfonyl)-2-(trifluoromethyl)phenoxy}-N,N-diethylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tungstate; dihydrogen peroxide; acetic acid / water / 1 h / 60 - 80 °C

2.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 0.25 h / Reflux

2.2: 1 h / 20 °C

2.3: 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 20 °C

With sodium tungstate; oxalyl dichloride; dihydrogen peroxide; sodium hydride; acetic acid; N,N-dimethyl-formamide; In dichloromethane; water; N,N-dimethyl-formamide; mineral oil;