tert-butyl(4-(4-(hydroxyldiphenylmethyl)piperidin-1-yl)-1-(4-isopropylphenyl)butan-1-oxy)dimethylsilane

Base Information

Chemical Name:tert-butyl(4-(4-(hydroxyldiphenylmethyl)piperidin-1-yl)-1-(4-isopropylphenyl)butan-1-oxy)dimethylsilane
CAS No.:1313731-46-2
Molecular Formula:C₃₇H₅₃NO₂Si
Molecular Weight:571.919
Hs Code.:

Synonyms:tert-butyl(4-(4-(hydroxyldiphenylmethyl)piperidin-1-yl)-1-(4-isopropylphenyl)butan-1-oxy)dimethylsilane

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Chemical Property of tert-butyl(4-(4-(hydroxyldiphenylmethyl)piperidin-1-yl)-1-(4-isopropylphenyl)butan-1-oxy)dimethylsilane

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Technology Process of tert-butyl(4-(4-(hydroxyldiphenylmethyl)piperidin-1-yl)-1-(4-isopropylphenyl)butan-1-oxy)dimethylsilane

There total 5 articles about tert-butyl(4-(4-(hydroxyldiphenylmethyl)piperidin-1-yl)-1-(4-isopropylphenyl)butan-1-oxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 4-(4'-(hydroxy(diphenyl)methyl)piperidin-1-yl)-1-(4-isopropylphenyl)butan-1-ol

: 1313731-46-2
tert-butyl(4-(4-(hydroxyldiphenylmethyl)piperidin-1-yl)-1-(4-isopropylphenyl)butan-1-oxy)dimethylsilane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 10.25h; Inert atmosphere;
DOI:10.1080/00397911.2010.502986

Reference yield:

: 115-46-8
C₁₈H₂₁NO

: 1313731-46-2
tert-butyl(4-(4-(hydroxyldiphenylmethyl)piperidin-1-yl)-1-(4-isopropylphenyl)butan-1-oxy)dimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydrogencarbonate / 5,5-dimethyl-1,3-cyclohexadiene; water / 12 h / Reflux

2: sodium tetrahydroborate / methanol / 0.5 h / Cooling with ice

3: 1H-imidazole / N,N-dimethyl-formamide / 10.25 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; potassium hydrogencarbonate; In methanol; 5,5-dimethyl-1,3-cyclohexadiene; water; N,N-dimethyl-formamide;
DOI:10.1080/00397911.2010.502986

Reference yield:

: 185066-40-4
4-(4'-(hydroxy(diphenyl)methyl)piperidin-1-yl)-1-(4-isopropylphenyl)butan-1-one

: 1313731-46-2
tert-butyl(4-(4-(hydroxyldiphenylmethyl)piperidin-1-yl)-1-(4-isopropylphenyl)butan-1-oxy)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 0.5 h / Cooling with ice

2: 1H-imidazole / N,N-dimethyl-formamide / 10.25 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; In methanol; N,N-dimethyl-formamide;
DOI:10.1080/00397911.2010.502986