dimethyl 4-[(4-methoxybenzyl)oxy]-1,4,5,6-tetrahydropyridine-1,2-dicarboxylate

Base Information

Chemical Name:dimethyl 4-[(4-methoxybenzyl)oxy]-1,4,5,6-tetrahydropyridine-1,2-dicarboxylate
CAS No.:1031883-63-2
Molecular Formula:C₁₇H₂₁NO₆
Molecular Weight:335.357
Hs Code.:

Synonyms:dimethyl 4-[(4-methoxybenzyl)oxy]-1,4,5,6-tetrahydropyridine-1,2-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl 4-[(4-methoxybenzyl)oxy]-1,4,5,6-tetrahydropyridine-1,2-dicarboxylate

Chemical Property:

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Technology Process of dimethyl 4-[(4-methoxybenzyl)oxy]-1,4,5,6-tetrahydropyridine-1,2-dicarboxylate

There total 1 articles about dimethyl 4-[(4-methoxybenzyl)oxy]-1,4,5,6-tetrahydropyridine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 1169758-58-0
C₂₇H₂₈NO₈P

: 1031883-63-2
dimethyl 4-[(4-methoxybenzyl)oxy]-1,4,5,6-tetrahydropyridine-1,2-dicarboxylate

Guidance literature:: With palladium diacetate; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide; at 50 ℃; for 2h;
DOI:10.1055/s-0028-1088202

Reference yield:

: 1031883-63-2
dimethyl 4-[(4-methoxybenzyl)oxy]-1,4,5,6-tetrahydropyridine-1,2-dicarboxylate

: dimethyl (2S,4R)-4-(4-methoxybenzyloxy)piperidine-1,2-dicarboxylate

: 1204587-94-9
dimethyl (2R,4R)-4-(4-methoxybenzyloxy)piperidine-1,2-dicarboxylate

Guidance literature:: With lithium triethylborohydride; In tetrahydrofuran; at 0 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1055/s-0029-1216979