1-benzyl-3-(2-picolyl)benzimidazolium hexafluorophosphate

Base Information

• Chemical Name: 1-benzyl-3-(2-picolyl)benzimidazolium hexafluorophosphate
• CAS No.: 1176334-04-5
• Molecular Formula: C₂₀H₁₈N₃*F₆P
• Molecular Weight: 445.347
• Mol file: 1176334-04-5.mol

Synonyms:1-benzyl-3-(2-picolyl)benzimidazolium hexafluorophosphate

Chemical Property of 1-benzyl-3-(2-picolyl)benzimidazolium hexafluorophosphate

Chemical Property:

Purity/Quality:

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Technology Process of 1-benzyl-3-(2-picolyl)benzimidazolium hexafluorophosphate

There total 4 articles about 1-benzyl-3-(2-picolyl)benzimidazolium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1-benzyl-3-(2-pyridylmethyl)-1H-benzimidazolium chloride (1176334-01-2) → 1-benzyl-3-(2-picolyl)benzimidazolium hexafluorophosphate (1176334-04-5)

Guidance literature:

With ammonium hexafluorophosphate; In water;

DOI:10.1016/j.jorganchem.2009.03.031

Reference yield: 81.0%

benzyl bromide (100-39-0) + 1-(pyridin-2-ylmethyl)-1H-benzo[d]imidazole (62154-64-7) → 1-benzyl-3-(2-picolyl)benzimidazolium hexafluorophosphate (1176334-04-5)

Guidance literature:

benzyl bromide; 1-(pyridin-2-ylmethyl)-1H-benzo[d]imidazole; In toluene; for 24h; Inert atmosphere; Reflux;

With ammonium hexafluorophosphate; In water; for 0.166667h;

DOI:10.1016/j.jorganchem.2017.07.016

Reference yield: 58.0%

1-benzylbenzimidazole (4981-92-4) + 2-chloromethylpyridine hydrochloride (6959-47-3) → 1-benzyl-3-(2-picolyl)benzimidazolium hexafluorophosphate (1176334-04-5)

Guidance literature:

With sodium hydrogencarbonate; In ethanol; for 28h; Reflux;

DOI:10.1016/j.ica.2011.12.007

upstream raw materials:

1-benzyl-3-(2-pyridylmethyl)-1H-benzimidazolium chloride

1-benzylbenzimidazole

2-chloromethylpyridine hydrochloride

benzyl bromide