1-benzyl-1-methoxycarbonylmethyl-4,4-bis(tert-butoxycarbonylmethyl)-1,4-diazabutane

Base Information

Chemical Name:1-benzyl-1-methoxycarbonylmethyl-4,4-bis(tert-butoxycarbonylmethyl)-1,4-diazabutane
CAS No.:1566605-70-6
Molecular Formula:C₂₄H₃₈N₂O₆
Molecular Weight:450.576
Hs Code.:

Synonyms:1-benzyl-1-methoxycarbonylmethyl-4,4-bis(tert-butoxycarbonylmethyl)-1,4-diazabutane

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Chemical Property of 1-benzyl-1-methoxycarbonylmethyl-4,4-bis(tert-butoxycarbonylmethyl)-1,4-diazabutane

Chemical Property:

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Technology Process of 1-benzyl-1-methoxycarbonylmethyl-4,4-bis(tert-butoxycarbonylmethyl)-1,4-diazabutane

There total 3 articles about 1-benzyl-1-methoxycarbonylmethyl-4,4-bis(tert-butoxycarbonylmethyl)-1,4-diazabutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17136-35-5
N-benzyl glycine methyl ester hydrochloride

: 146432-43-1
N-(2-bromoethyl)-N-[2-(1,1-dimethylethoxy)-2-oxoethyl]glycine 1,1-dimethylethyl ester

: 1566605-70-6
1-benzyl-1-methoxycarbonylmethyl-4,4-bis(tert-butoxycarbonylmethyl)-1,4-diazabutane

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 16h;
DOI:10.1021/ol500022n

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1566605-70-6
1-benzyl-1-methoxycarbonylmethyl-4,4-bis(tert-butoxycarbonylmethyl)-1,4-diazabutane

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 0.16 h / 0 - 20 °C

2: N-Bromosuccinimide; triphenylphosphine / dichloromethane / 2.08 h / 0 °C

3: potassium carbonate / acetonitrile / 16 h / 20 °C

With N-Bromosuccinimide; potassium carbonate; potassium hydrogencarbonate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol500022n

Reference yield:

: 146432-41-9
[tert-Butoxycarbonylmethyl-(2-hydroxy-ethyl)-amino]-acetic acid tert-butyl ester

: 1566605-70-6
1-benzyl-1-methoxycarbonylmethyl-4,4-bis(tert-butoxycarbonylmethyl)-1,4-diazabutane

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; triphenylphosphine / dichloromethane / 2.08 h / 0 °C

2: potassium carbonate / acetonitrile / 16 h / 20 °C

With N-Bromosuccinimide; potassium carbonate; triphenylphosphine; In dichloromethane; acetonitrile;
DOI:10.1021/ol500022n