1-<2-<2-<(tert-butyldiphenylsilyl)oxy>ethyl>-4,5-dimethoxyphenyl>-2-(3,4-dimethoxyphenyl)ethylamine

Base Information

• Chemical Name: 1-<2-<2-<(tert-butyldiphenylsilyl)oxy>ethyl>-4,5-dimethoxyphenyl>-2-(3,4-dimethoxyphenyl)ethylamine
• CAS No.: 173030-97-2
• Molecular Formula: C₃₆H₄₅NO₅Si
• Molecular Weight: 599.842

Synonyms:1-<2-<2-<(tert-butyldiphenylsilyl)oxy>ethyl>-4,5-dimethoxyphenyl>-2-(3,4-dimethoxyphenyl)ethylamine

Chemical Property of 1-<2-<2-<(tert-butyldiphenylsilyl)oxy>ethyl>-4,5-dimethoxyphenyl>-2-(3,4-dimethoxyphenyl)ethylamine

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Technology Process of 1-<2-<2-<(tert-butyldiphenylsilyl)oxy>ethyl>-4,5-dimethoxyphenyl>-2-(3,4-dimethoxyphenyl)ethylamine

There total 1 articles about 1-<2-<2-<(tert-butyldiphenylsilyl)oxy>ethyl>-4,5-dimethoxyphenyl>-2-(3,4-dimethoxyphenyl)ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethanone oxime → 1-<2-<2-<(tert-butyldiphenylsilyl)oxy>ethyl>-4,5-dimethoxyphenyl>-2-(3,4-dimethoxyphenyl)ethylamine (173030-97-2)

Guidance literature:

With sodium tetrahydroborate; titanium tetrachloride; In 1,2-dimethoxyethane; for 14h; Ambient temperature;

DOI:10.1021/jo960007s

Reference yield: 89.0%

benzoyl chloride (98-88-4) + 1-<2-<2-<(tert-butyldiphenylsilyl)oxy>ethyl>-4,5-dimethoxyphenyl>-2-(3,4-dimethoxyphenyl)ethylamine (173030-97-2) → N-[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-benzamide (177726-12-4)

Guidance literature:

With dmap; triethylamine; In dichloromethane; for 4h; Ambient temperature;

DOI:10.1021/jo960007s

Reference yield: 85.0%

acetyl chloride (75-36-5) + 1-<2-<2-<(tert-butyldiphenylsilyl)oxy>ethyl>-4,5-dimethoxyphenyl>-2-(3,4-dimethoxyphenyl)ethylamine (173030-97-2) → N-[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide (177726-02-2)

Guidance literature:

With dmap; triethylamine; In dichloromethane; for 4h; Ambient temperature;

DOI:10.1021/jo960007s

Downstream raw materials:

[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-methoxymethyl-amine

3-<2-(2-t-butyldiphenylsilyloxyethyl)-4,5-dimethoxyphenyl>-6,7-dimethoxytetrahydroisoquinoline

N-[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-benzamide

N-[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide

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