7-benzoylamino-6-methyl-[1,3]dioxolo[4,5-g]quinazolinium betaine

Base Information

• Chemical Name: 7-benzoylamino-6-methyl-[1,3]dioxolo[4,5-g]quinazolinium betaine
• CAS No.: 57492-77-0
• Molecular Formula: C₁₇H₁₃N₃O₃
• Molecular Weight: 307.309
• Mol file: 57492-77-0.mol

Synonyms:7-benzoylamino-6-methyl-[1,3]dioxolo[4,5-g]quinazolinium betaine

Chemical Property of 7-benzoylamino-6-methyl-[1,3]dioxolo[4,5-g]quinazolinium betaine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7-benzoylamino-6-methyl-[1,3]dioxolo[4,5-g]quinazolinium betaine

There total 2 articles about 7-benzoylamino-6-methyl-[1,3]dioxolo[4,5-g]quinazolinium betaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(8-methoxy-6-methyl-8H-[1,3]dioxolo[4,5-g]quinazolin-7-yl)-benzamide; hydrochloride (58277-09-1) → 7-benzoylamino-6-methyl-[1,3]dioxolo[4,5-g]quinazolinium betaine (57492-77-0)

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.1016/0040-4020(75)80270-5

Reference yield:

7-benzoylamino-6-methyl-7,8-dihydro-[1,3]dioxolo[4,5-g]quinazolin-8-ol (58277-10-4) → 7-benzoylamino-6-methyl-[1,3]dioxolo[4,5-g]quinazolinium betaine (57492-77-0)

Guidance literature:

In benzene;

DOI:10.1016/0040-4020(75)80270-5

Reference yield: 68.0%

7-benzoylamino-6-methyl-[1,3]dioxolo[4,5-g]quinazolinium betaine (57492-77-0) + acetone (67-64-1) → N-[6-Methyl-8-(2-oxo-propyl)-8H-[1,3]dioxolo[4,5-g]quinazolin-7-yl]-benzamide (80056-18-4)

Guidance literature:

With N-butylamine; Ambient temperature;

upstream raw materials:

N-(8-methoxy-6-methyl-8H-[1,3]dioxolo[4,5-g]quinazolin-7-yl)-benzamide; hydrochloride

7-benzoylamino-6-methyl-7,8-dihydro-[1,3]dioxolo[4,5-g]quinazolin-8-ol

Downstream raw materials:

7-benzoylamino-6-methyl-7H-[1,3]dioxolo[4,5-g]quinazoline-8-thione

benzoylhydrazone of benzaldehyde

benzamide

benzoic acid hydrazide