1-(2,6-diisopropylphenyl)-3-methyl imidazolium iodide

Base Information

Chemical Name:1-(2,6-diisopropylphenyl)-3-methyl imidazolium iodide
CAS No.:852057-21-7
Molecular Formula:C₁₆H₂₃N₂*I
Molecular Weight:370.277
Hs Code.:

Synonyms:1-(2,6-diisopropylphenyl)-3-methyl imidazolium iodide

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Chemical Property of 1-(2,6-diisopropylphenyl)-3-methyl imidazolium iodide

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Technology Process of 1-(2,6-diisopropylphenyl)-3-methyl imidazolium iodide

There total 1 articles about 1-(2,6-diisopropylphenyl)-3-methyl imidazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 25364-47-0
1-(2,6-diisopropylphenyl)-1H-imidazole

: 74-88-4
methyl iodide

: 852057-21-7
1-(2,6-diisopropylphenyl)-3-methyl imidazolium iodide

Guidance literature:: In dichloromethane; at 30 - 35 ℃; for 16h;
DOI:10.1016/j.jorganchem.2007.10.012

Reference yield: 91.0%

: 852057-21-7
1-(2,6-diisopropylphenyl)-3-methyl imidazolium iodide

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: bis(1-[2,6-bis(1-methylethyl)phenyl]-1,3-dihydro-3-methyl-2-H-imidazol-2-ylidene)copper⁽¹⁺⁾ hexafluorophosphate^(1-) (1:1)

Guidance literature:: With KOC(CH₃)3; In tetrahydrofuran; (Ar); to soln. of imidazolium salt in THF was added KO(t)Bu and copper complex, stirred at room temp. for 12 h; filtered through celite, filtrate was evapd., washed with Et2O, precipitated from THF by addition of Et2O, elem. anal.;
DOI:10.1002/hlca.200800406

Reference yield: 91.0%

: 852057-21-7
1-(2,6-diisopropylphenyl)-3-methyl imidazolium iodide

: 20667-12-3
silver(l) oxide

: 1-(2,6-diisopropylphenyl)-3-methyl-imidazol-2-ylidene silver iodide

Guidance literature:: In dichloromethane; (Ar), Ag2O added to soln. of 2 equiv. of ligand in CH2Cl2, stirred at 20°C for 5.5 h (exclusion of light); filtered, concd.(vac.), dried (vac.);
DOI:10.1002/ejic.200801157