(Z)-2-(1-(4-chlorophenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(Z)-2-(1-(4-chlorophenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1446696-28-1
Molecular Formula:C₁₅H₂₀BClO₂
Molecular Weight:278.587
Hs Code.:

Synonyms:(Z)-2-(1-(4-chlorophenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(1-(4-chlorophenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (Z)-2-(1-(4-chlorophenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 8 articles about (Z)-2-(1-(4-chlorophenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2749-97-5
4-methoxylphenylallene

: 73183-34-3
bis(pinacol)diborane

: 1446696-28-1
(Z)-2-(1-(4-chlorophenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 2-(3-(4-methoxyphenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: bis(pinacol)diborane; With [CuCl(IMes^Me)]; sodium t-butanolate; In toluene; at 20 ℃; for 0.0833333h; Inert atmosphere;

4-methoxylphenylallene; With 1,1,1,3',3',3'-hexafluoro-propanol; In toluene; at -20 ℃; for 2h; regioselective reaction; Inert atmosphere;
DOI:10.1002/chem.201300443

Reference yield:

: 2809-65-6
4-chloro-1-propynylbenzene

: 73183-34-3
bis(pinacol)diborane

: 1446696-28-1
(Z)-2-(1-(4-chlorophenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: bis(pinacol)diborane; With triphenylphosphine; copper(l) chloride; sodium t-butanolate; In tetrahydrofuran; at 20 ℃; for 0.166667h; Schlenk technique; Inert atmosphere;

4-chloro-1-propynylbenzene; In tetrahydrofuran; methanol; at 20 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1002/chem.202000703

Reference yield:

: 2749-98-6
4-chlorophenylallene

: 73183-34-3
bis(pinacol)diborane

: 1402235-32-8
2-(3-(4-chlorophenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1446696-28-1
(Z)-2-(1-(4-chlorophenyl)prop-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With copper(II) sulfate; triphenylphosphine; benzylamine; In water; at 20 ℃; for 3h; Overall yield = 87 percent; Inert atmosphere;
DOI:10.1039/d0nj02010a