isopropyl 3-(((6-(-2-(dimethylamino)-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)amino)methyl)benzoate

Base Information

Chemical Name:isopropyl 3-(((6-(-2-(dimethylamino)-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)amino)methyl)benzoate
CAS No.:1351956-66-5
Molecular Formula:C₂₇H₃₃N₅O₂S
Molecular Weight:491.657
Hs Code.:

Synonyms:isopropyl 3-(((6-(-2-(dimethylamino)-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)amino)methyl)benzoate

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Chemical Property of isopropyl 3-(((6-(-2-(dimethylamino)-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)amino)methyl)benzoate

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Technology Process of isopropyl 3-(((6-(-2-(dimethylamino)-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)amino)methyl)benzoate

There total 8 articles about isopropyl 3-(((6-(-2-(dimethylamino)-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)amino)methyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 546-68-9
titanium(IV) isopropylate

: 1351956-54-1
6-(2-(dimethylamino)-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-amine

: 52178-50-4
Methyl 3-formylbenzoate

: 1351956-65-4
methyl 3-(((6-(-2-(dimethylamino)-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)amino)methyl)benzoate

: 1351956-66-5
isopropyl 3-(((6-(-2-(dimethylamino)-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)amino)methyl)benzoate

Guidance literature:: titanium(IV) isopropylate; 6-(2-(dimethylamino)-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-amine; Methyl 3-formylbenzoate; In tetrahydrofuran; at 20 ℃;

With sodium tetrahydroborate; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 1351956-60-9
4-(2-(dimethylamino)-1-(1H-imidazol-1-yl)butyl)aniline

: 1351956-66-5
isopropyl 3-(((6-(-2-(dimethylamino)-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)amino)methyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: bromine; acetic acid / 1 h / 7 - 20 °C

2.1: tetrahydrofuran / 20 °C

2.2: 1 h / 20 °C

With bromine; acetic acid; In tetrahydrofuran;

Reference yield:

: 13211-00-2
N-(4-butyrylphenyl)acetamide

: 1351956-66-5
isopropyl 3-(((6-(-2-(dimethylamino)-1-(1H-imidazol-1-yl)butyl)benzo[d]thiazol-2-yl)amino)methyl)benzoate

Guidance literature:: Multi-step reaction with 7 steps

1.1: aluminum (III) chloride; bromine / dichloromethane / 3.5 h / 0 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / chloroform; methanol / 48 h / 20 °C

3.1: sodium tetrahydroborate; methanol / 20 °C / Inert atmosphere; Cooling with ice

4.1: acetonitrile / Reflux

5.1: hydrogenchloride / water / 60 °C

6.1: bromine; acetic acid / 1 h / 7 - 20 °C

7.1: tetrahydrofuran / 20 °C

7.2: 1 h / 20 °C

With hydrogenchloride; methanol; aluminum (III) chloride; sodium tetrahydroborate; bromine; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; acetonitrile;