C₂₇H₃₄N₂O₃

Base Information

Chemical Name:C₂₇H₃₄N₂O₃
CAS No.:1394050-37-3
Molecular Formula:C₂₇H₃₄N₂O₃
Molecular Weight:434.579
Hs Code.:

C<sub>27</sub>H<sub>34</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₇H₃₄N₂O₃

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Chemical Property of C₂₇H₃₄N₂O₃

Chemical Property:

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Technology Process of C₂₇H₃₄N₂O₃

There total 13 articles about C₂₇H₃₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 5815-08-7
tert-Butoxybis(dimethylamino)methane

: 1383029-27-3
(S)-2-(1-biphenyl-4-yl-1-methylethyl)-5-oxo-pyrrolidine-1-carboxylic acid t-butyl ester

: 1394050-37-3
C₂₇H₃₄N₂O₃

Guidance literature:: at 80 ℃; for 3h;

Reference yield:

: 676627-65-9
C₁₁H₁₄BrNO₂

: 1394050-37-3
C₂₇H₃₄N₂O₃

Guidance literature:: Multi-step reaction with 10 steps

1: triethylamine / dichloromethane / 0 °C / Reflux

2: sodium hydroxide / methanol / 4 h / 20 °C

3: lithium hydroxide / water / 60 h / 37 °C / pH 8.5

4: hydrogenchloride; water / Reflux

5: water; acetone / 2 h / 20 °C

6: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 8 h / 75 °C / Inert atmosphere

7: dmap; dicyclohexyl-carbodiimide / dichloromethane / -5 °C

8: sodium tetrahydroborate; acetic acid / dichloromethane / 3.5 h / -5 °C / Inert atmosphere

9: toluene / 3 h / Reflux

10: 3 h / 80 °C

With hydrogenchloride; dmap; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; potassium carbonate; acetic acid; triethylamine; dicyclohexyl-carbodiimide; sodium hydroxide; lithium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; acetone; toluene;

Reference yield:

: 32454-16-3
2-(4-bromophenyl)-2-methyl-propionaldehyde

: 1394050-37-3
C₂₇H₃₄N₂O₃

Guidance literature:: Multi-step reaction with 12 steps

1: ammonium carbonate / water / Reflux

2: sodium hydroxide / ethylene glycol / 38 h / 120 °C

3: triethylamine / dichloromethane / 0 °C / Reflux

4: sodium hydroxide / methanol / 4 h / 20 °C

5: lithium hydroxide / water / 60 h / 37 °C / pH 8.5

6: hydrogenchloride; water / Reflux

7: water; acetone / 2 h / 20 °C

8: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 8 h / 75 °C / Inert atmosphere

9: dmap; dicyclohexyl-carbodiimide / dichloromethane / -5 °C

10: sodium tetrahydroborate; acetic acid / dichloromethane / 3.5 h / -5 °C / Inert atmosphere

11: toluene / 3 h / Reflux

12: 3 h / 80 °C

With hydrogenchloride; dmap; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; ammonium carbonate; potassium carbonate; acetic acid; triethylamine; dicyclohexyl-carbodiimide; sodium hydroxide; lithium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; ethylene glycol; acetone; toluene;