[3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl]-[3,5-bis(4-methoxyphenyl)pyrrol-2-ylidene]amine

Base Information

• Chemical Name: [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl]-[3,5-bis(4-methoxyphenyl)pyrrol-2-ylidene]amine
• CAS No.: 873975-75-8
• Molecular Formula: C₃₆H₃₁N₃O₄
• Molecular Weight: 569.66
• Mol file: 873975-75-8.mol

Synonyms:[3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl]-[3,5-bis(4-methoxyphenyl)pyrrol-2-ylidene]amine

Chemical Property of [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl]-[3,5-bis(4-methoxyphenyl)pyrrol-2-ylidene]amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl]-[3,5-bis(4-methoxyphenyl)pyrrol-2-ylidene]amine

There total 4 articles about [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl]-[3,5-bis(4-methoxyphenyl)pyrrol-2-ylidene]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-bis(4-methoxyphenyl)-4-nitrobutan-1-one (101730-62-5) → [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl]-[3,5-bis(4-methoxyphenyl)pyrrol-2-ylidene]amine (873975-75-8)

Guidance literature:

With ammonium acetate; In ethanol; at 80 ℃; for 24h;

DOI:10.1039/d0pp00114g

Reference yield:

4,4'-dimethoxychalcone (2373-89-9) → [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl]-[3,5-bis(4-methoxyphenyl)pyrrol-2-ylidene]amine (873975-75-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 2 h / 20 °C

2: ammonium acetate / ethanol / 24 h / 80 °C

With ammonium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In ethanol;

DOI:10.1039/d0pp00114g

Reference yield:

1-(4-methoxyphenyl)ethanone (100-06-1) → [3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl]-[3,5-bis(4-methoxyphenyl)pyrrol-2-ylidene]amine (873975-75-8)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydroxide / methanol / 2 h / 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / 2 h / 20 °C

3: ammonium acetate / ethanol / 24 h / 80 °C

With ammonium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium hydroxide; In methanol; ethanol;

DOI:10.1039/d0pp00114g

upstream raw materials:

4,4'-dimethoxychalcone

1-(4-methoxyphenyl)ethanone

4-methoxy-benzaldehyde

1,3-bis(4-methoxyphenyl)-4-nitrobutan-1-one

Downstream raw materials:

[3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]BF₂

bis[3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]zinc(II)

bis[3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]copper(II)

bis[3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]nickel(II)