4-Methoxy-4-phenyl-2,5-cyclohexadienone N-acetylimine

Base Information

Chemical Name:4-Methoxy-4-phenyl-2,5-cyclohexadienone N-acetylimine
CAS No.:146474-21-7
Molecular Formula:C₁₅H₁₅NO₂
Molecular Weight:241.29
Hs Code.:

Synonyms:4-Methoxy-4-phenyl-2,5-cyclohexadienone N-acetylimine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Methoxy-4-phenyl-2,5-cyclohexadienone N-acetylimine

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Technology Process of 4-Methoxy-4-phenyl-2,5-cyclohexadienone N-acetylimine

There total 5 articles about 4-Methoxy-4-phenyl-2,5-cyclohexadienone N-acetylimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 67-56-1
methanol

: 4075-79-0
4-phenylacetanilide

: 28093-86-9
1-methoxy-4-(phenylethynyl)-1,4-dihydro-[1,1'-biphenyl]-4-ol

: 146474-21-7
4-Methoxy-4-phenyl-2,5-cyclohexadienone N-acetylimine

Guidance literature:: With lithium perchlorate; sodium hydrogencarbonate; In water; at 0 ℃; for 0.7h; anodic oxidation;
DOI:10.1021/jo00056a019

Reference yield:

: 92-67-1
4-phenylalanine

: 146474-21-7
4-Methoxy-4-phenyl-2,5-cyclohexadienone N-acetylimine

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / n-BuLi / tetrahydrofuran / 0.5 h / 0 °C

2: 72 percent / imidazole / tetrahydrofuran / 1 h

3: 45 percent / NaHCO₃ / H₂O / 1.5 h / 0 °C / single-cell anodic oxidation, platinum electrodes, a constant current 0.15 A, LiClO₄ as supporting electrolyte

With 1H-imidazole; n-butyllithium; sodium hydrogencarbonate; In tetrahydrofuran; water;
DOI:10.1021/jo00073a016

Reference yield:

: 151965-78-5
N-<2-(Hydroxymethyl)benzoyl>-4-aminobiphenyl

: 146474-21-7
4-Methoxy-4-phenyl-2,5-cyclohexadienone N-acetylimine

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / imidazole / tetrahydrofuran / 1 h

2: 45 percent / NaHCO₃ / H₂O / 1.5 h / 0 °C / single-cell anodic oxidation, platinum electrodes, a constant current 0.15 A, LiClO₄ as supporting electrolyte

With 1H-imidazole; sodium hydrogencarbonate; In tetrahydrofuran; water;
DOI:10.1021/jo00073a016