2-bromo-2′,2″-diiodotriphenylmethane

Base Information

Chemical Name:2-bromo-2′,2″-diiodotriphenylmethane
CAS No.:1534332-88-1
Molecular Formula:C₁₉H₁₃BrI₂
Molecular Weight:575.025
Hs Code.:

Synonyms:2-bromo-2′,2″-diiodotriphenylmethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromo-2′,2″-diiodotriphenylmethane

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Technology Process of 2-bromo-2′,2″-diiodotriphenylmethane

There total 7 articles about 2-bromo-2′,2″-diiodotriphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1534332-87-0
10-(2-bromophenyl)-10H-dibenzo[b,e]iodininium iodide

: 1534332-88-1
2-bromo-2′,2″-diiodotriphenylmethane

Guidance literature:: at 200 ℃; for 0.25h; Schlenk technique; Inert atmosphere;
DOI:10.1021/ja4114962

Reference yield:

: 1534332-86-9
1-bromo-2-((2-iodophenyl)(phenyl)methyl)benzene

: 1534332-88-1
2-bromo-2′,2″-diiodotriphenylmethane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

1.2: 255 / 1.08 h / 20 °C / Inert atmosphere

1.3: 0.08 h

2.1: 0.25 h / 200 °C / Schlenk technique; Inert atmosphere

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/ja4114962

Reference yield:

: 1534332-85-8
10-phenyl-10H-dibenzo[b,e]iodininium bromide

: 1534332-88-1
2-bromo-2′,2″-diiodotriphenylmethane

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutylammomium bromide; copper(I) bromide / acetonitrile / 120 h / Reflux; Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

2.2: 255 / 1.08 h / 20 °C / Inert atmosphere

2.3: 0.08 h

3.1: 0.25 h / 200 °C / Schlenk technique; Inert atmosphere

With tetrabutylammomium bromide; 3-chloro-benzenecarboperoxoic acid; copper(I) bromide; In dichloromethane; acetonitrile;
DOI:10.1021/ja4114962