(1,2-dimethyl-3-indolyl)(4-methoxyphenyl)methylium o-benzenedisulfonimide

Base Information

Chemical Name:(1,2-dimethyl-3-indolyl)(4-methoxyphenyl)methylium o-benzenedisulfonimide
CAS No.:1373513-48-4
Molecular Formula:C₆H₄NO₄S₂*C₁₈H₁₈NO
Molecular Weight:482.581
Hs Code.:

Synonyms:(1,2-dimethyl-3-indolyl)(4-methoxyphenyl)methylium o-benzenedisulfonimide

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Chemical Property of (1,2-dimethyl-3-indolyl)(4-methoxyphenyl)methylium o-benzenedisulfonimide

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Technology Process of (1,2-dimethyl-3-indolyl)(4-methoxyphenyl)methylium o-benzenedisulfonimide

There total 1 articles about (1,2-dimethyl-3-indolyl)(4-methoxyphenyl)methylium o-benzenedisulfonimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 875-79-6
1,2-dimethylindole

: 4482-01-3
o-benzenedisulfonimide

: 123-11-5
4-methoxy-benzaldehyde

: 1373513-48-4
(1,2-dimethyl-3-indolyl)(4-methoxyphenyl)methylium o-benzenedisulfonimide

Guidance literature:: In acetonitrile; at 20 - 25 ℃; for 0.5h;
DOI:10.1021/jo300099y

Reference yield: 94.0%

: 1373513-48-4
(1,2-dimethyl-3-indolyl)(4-methoxyphenyl)methylium o-benzenedisulfonimide

: 1373513-54-2
(4-methoxyphenyl)(1,2-dimethyl-3-indolyl)methane

Guidance literature:: With sodium tetrahydroborate; In acetonitrile; at 20 - 25 ℃; for 0.166667h;
DOI:10.1021/jo300099y

Reference yield:

: 6651-36-1
1-(Trimethylsilyloxy)cyclohexene

: 1373513-48-4
(1,2-dimethyl-3-indolyl)(4-methoxyphenyl)methylium o-benzenedisulfonimide

: 2-[(4-methoxyphenyl)(1,2-dimethyl-3-indolyl)methyl]cyclohexanone

: 2-[(4-methoxyphenyl)(1,2-dimethyl-3-indolyl)methyl]cyclohexanone

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; at 20 - 25 ℃; for 24h; Overall yield = 62 %; Optical yield = 52 %de; diastereoselective reaction;
DOI:10.1016/j.tetlet.2016.09.042