(6S,9S,15S)-methyl 6,9-dibenzyl-15-((R)-1-hydroxyethyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

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Chemical Name:(6S,9S,15S)-methyl 6,9-dibenzyl-15-((R)-1-hydroxyethyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate
CAS No.:1620161-90-1
Molecular Formula:C₃₀H₄₀N₄O₈
Molecular Weight:584.67
Hs Code.:

Synonyms:(6S,9S,15S)-methyl 6,9-dibenzyl-15-((R)-1-hydroxyethyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

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Chemical Property of (6S,9S,15S)-methyl 6,9-dibenzyl-15-((R)-1-hydroxyethyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

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Technology Process of (6S,9S,15S)-methyl 6,9-dibenzyl-15-((R)-1-hydroxyethyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

There total 2 articles about (6S,9S,15S)-methyl 6,9-dibenzyl-15-((R)-1-hydroxyethyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 3373-59-9
L-threonine methyl ester

: 1620161-82-1
(6S,9S)-S-4-nitrophenyl 6,9-dibenzyl-2,2-dimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecane-13-thioate

: 1620161-90-1
(6S,9S,15S)-methyl 6,9-dibenzyl-15-((R)-1-hydroxyethyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

Guidance literature:: With sodium hydrogencarbonate; In dimethyl sulfoxide; at 20 ℃; for 25h; Inert atmosphere;
DOI:10.1021/ol501669n

Reference yield:

: 82816-76-0
N-tert-butoxycarbonyl-L-phenylalanine-L-phenylalanine-glycine

: 1620161-90-1
(6S,9S,15S)-methyl 6,9-dibenzyl-15-((R)-1-hydroxyethyl)-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: sodium hydrogencarbonate / dimethyl sulfoxide / 25 h / 20 °C / Inert atmosphere

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ol501669n