1,5-diphenyl-3-methyl-7-(1,4,6-trimethyl-1,4-diazacycloheptane-6-yl)diazabicyclo[3.3.1]nonane-9-one

Base Information

• Chemical Name: 1,5-diphenyl-3-methyl-7-(1,4,6-trimethyl-1,4-diazacycloheptane-6-yl)diazabicyclo[3.3.1]nonane-9-one
• CAS No.: 1101929-27-4
• Molecular Formula: C₂₈H₃₈N₄O
• Molecular Weight: 446.636

Synonyms:1,5-diphenyl-3-methyl-7-(1,4,6-trimethyl-1,4-diazacycloheptane-6-yl)diazabicyclo[3.3.1]nonane-9-one

Chemical Property of 1,5-diphenyl-3-methyl-7-(1,4,6-trimethyl-1,4-diazacycloheptane-6-yl)diazabicyclo[3.3.1]nonane-9-one

Chemical Property:

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Technology Process of 1,5-diphenyl-3-methyl-7-(1,4,6-trimethyl-1,4-diazacycloheptane-6-yl)diazabicyclo[3.3.1]nonane-9-one

There total 1 articles about 1,5-diphenyl-3-methyl-7-(1,4,6-trimethyl-1,4-diazacycloheptane-6-yl)diazabicyclo[3.3.1]nonane-9-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.4%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1-(1,4,6-trimethyl-1,4-diazacycloheptane-6-yl)-3,5-diphenylpiperidine-4-one (1101929-26-3) + methylamine (74-89-5) → 1,5-diphenyl-3-methyl-7-(1,4,6-trimethyl-1,4-diazacycloheptane-6-yl)diazabicyclo[3.3.1]nonane-9-one (1101929-27-4)

Guidance literature:

With acetic acid; In methanol; at 0 - 65 ℃;

Reference yield: 73.0%

1,5-diphenyl-3-methyl-7-(1,4,6-trimethyl-1,4-diazacycloheptane-6-yl)diazabicyclo[3.3.1]nonane-9-one (1101929-27-4) + cobalt(II) perchlorate hexahydrate + acetonitrile (75-05-8,26809-02-9) → Co((CH3)3C5H8N2C7H8N2(C6H5)2(O)CH3)(NCCH3)(2+)*2ClO4(1-)=[Co((CH3)3C5H8N2C7H8N2(C6H5)2(O)CH3)(NCCH3)](ClO4)2

Guidance literature:

In acetonitrile; soln. of Co salt in MeCN added to soln. of bispidine deriv. in MeCN, mixt. stirred at room temp. overnight; evapn. (vac.), residue dissolved in MeCN, slow diffusion of Et2O into soln.; elem. anal.;

DOI:10.1021/ic900571v

Reference yield: 55.2%

1,5-diphenyl-3-methyl-7-(1,4,6-trimethyl-1,4-diazacycloheptane-6-yl)diazabicyclo[3.3.1]nonane-9-one (1101929-27-4) → 2BF4(1-)*C30H42CuN5O(2+)

Guidance literature:

With copper(II) bis(tetrafluoroborate); In acetonitrile; at 20 - 82 ℃;

upstream raw materials:

formaldehyd

1-(1,4,6-trimethyl-1,4-diazacycloheptane-6-yl)-3,5-diphenylpiperidine-4-one

methylamine

Downstream raw materials:

Cu⁽¹⁺⁾*C₂H₄N₂(CH₃)2C₂H₄CCH₃NC₂H₄C₂COC₂H₄NCH₃(C₆H₅)2*B(C₆F₅)4^(1-)=Cu(C₄H₈N₂(CH₃)3CNC₄H₈C₂CONCH₃(C₆H₅)2)(B(C₆F₅)4)

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