3,3,6,6-tetramethyl-1,8-dioxo-9-(4-methoxyphenyl)-10-(4-phenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine

Base Information

• Chemical Name: 3,3,6,6-tetramethyl-1,8-dioxo-9-(4-methoxyphenyl)-10-(4-phenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine
• CAS No.: 159301-95-8
• Molecular Formula: C₃₀H₃₃NO₃
• Molecular Weight: 455.597

Synonyms:3,3,6,6-tetramethyl-1,8-dioxo-9-(4-methoxyphenyl)-10-(4-phenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine

Chemical Property of 3,3,6,6-tetramethyl-1,8-dioxo-9-(4-methoxyphenyl)-10-(4-phenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine

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Technology Process of 3,3,6,6-tetramethyl-1,8-dioxo-9-(4-methoxyphenyl)-10-(4-phenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine

There total 8 articles about 3,3,6,6-tetramethyl-1,8-dioxo-9-(4-methoxyphenyl)-10-(4-phenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-methoxy-benzaldehyde (123-11-5) + dimedone (126-81-8) + aniline (62-53-3) → 3,3,6,6-tetramethyl-1,8-dioxo-9-(4-methoxyphenyl)-10-(4-phenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine (159301-95-8)

Guidance literature:

With polyvinylpolypyrrolidone supported boron trifluoride; In acetonitrile; for 3.5h; Reflux;

DOI:10.1007/s00706-014-1206-9

Reference yield: 79.0%

5,5-dimethyl-3-(phenylamino)cyclohex-2-en-1-one (18940-21-1) + 4-methoxy-benzaldehyde (123-11-5) → 3,3,6,6-tetramethyl-1,8-dioxo-9-(4-methoxyphenyl)-10-(4-phenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine (159301-95-8)

Guidance literature:

With phosphorus pentoxide; In isopropyl alcohol; Heating;

DOI:10.1023/A:1013845426393

Reference yield: 75.0%

5,5-dimethyl-3-(phenylamino)cyclohex-2-en-1-one (18940-21-1) + dimedone (126-81-8) + 4-Methoxybenzyl alcohol (105-13-5) → 3,3,6,6-tetramethyl-1,8-dioxo-9-(4-methoxyphenyl)-10-(4-phenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine (159301-95-8)

Guidance literature:

With potassium tert-butylate; C₃₇H₃₇Cl₂NPRuS₂; at 135 ℃; for 36h; Inert atmosphere;

DOI:10.1021/acs.joc.1c01075

upstream raw materials:

5,5-dimethyl-3-(phenylamino)cyclohex-2-en-1-one

4-methoxy-benzaldehyde

dimedone

aniline

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