(10,10-dimethyl-2-oxo-3-phenyl-3,4-diazatricyclo[5.2.1.0^1,5]dec-4-yl)-oxoacetaldehyde

Base Information

• Chemical Name: (10,10-dimethyl-2-oxo-3-phenyl-3,4-diazatricyclo[5.2.1.0^1,5]dec-4-yl)-oxoacetaldehyde
• CAS No.: 682806-82-2
• Molecular Formula: C₁₈H₂₀N₂O₃
• Molecular Weight: 312.368

Synonyms:(10,10-dimethyl-2-oxo-3-phenyl-3,4-diazatricyclo[5.2.1.0^1,5]dec-4-yl)-oxoacetaldehyde

Chemical Property of (10,10-dimethyl-2-oxo-3-phenyl-3,4-diazatricyclo[5.2.1.0^1,5]dec-4-yl)-oxoacetaldehyde

Chemical Property:

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Technology Process of (10,10-dimethyl-2-oxo-3-phenyl-3,4-diazatricyclo[5.2.1.0^1,5]dec-4-yl)-oxoacetaldehyde

There total 1 articles about (10,10-dimethyl-2-oxo-3-phenyl-3,4-diazatricyclo[5.2.1.0^1,5]dec-4-yl)-oxoacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

oxalyl dichloride (79-37-8) + 7,7-dimethyl-2'-phenyl-pyrazol-3'-one-bicyclo[2.2.1]heptane (263722-72-1) → (10,10-dimethyl-2-oxo-3-phenyl-3,4-diazatricyclo[5.2.1.01,5]dec-4-yl)-oxoacetaldehyde (682806-82-2)

Guidance literature:

oxalyl dichloride; 7,7-dimethyl-2'-phenyl-pyrazol-3'-one-bicyclo[2.2.1]heptane; In dichloromethane; at 20 ℃;

With tri-n-butyl-tin hydride; In benzene; at 20 ℃; for 0.166667h; Further stages.;

DOI:10.1016/j.tetlet.2004.02.001

Reference yield: 87.0%

isopropenylbenzene (98-83-9,6144-04-3,25014-31-7,42612-14-6) + (10,10-dimethyl-2-oxo-3-phenyl-3,4-diazatricyclo[5.2.1.01,5]dec-4-yl)-oxoacetaldehyde (682806-82-2) → (1S,5R,7R)-4-(2-Hydroxy-4-phenyl-pent-4-enoyl)-10,10-dimethyl-3-phenyl-3,4-diaza-tricyclo[5.2.1.01,5]decan-2-one

Guidance literature:

With scandium tris(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 24h;

DOI:10.1016/j.tetlet.2004.10.121

Reference yield: 85.0%

1-chloro-4-(1-methylethenyl)-benzene (1712-70-5) + (10,10-dimethyl-2-oxo-3-phenyl-3,4-diazatricyclo[5.2.1.01,5]dec-4-yl)-oxoacetaldehyde (682806-82-2) → (1S,5R,7R)-4-[4-(4-Chloro-phenyl)-2-hydroxy-pent-4-enoyl]-10,10-dimethyl-3-phenyl-3,4-diaza-tricyclo[5.2.1.01,5]decan-2-one

Guidance literature:

With scandium tris(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 24h;

DOI:10.1016/j.tetlet.2004.10.121

upstream raw materials:

oxalyl dichloride

7,7-dimethyl-2'-phenyl-pyrazol-3'-one-bicyclo[2.2.1]heptane

Downstream raw materials:

(S)-4-((1S,5R,7R)-10,10-Dimethyl-2-oxo-3-phenyl-3,4-diaza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-hydroxy-2-methylene-4-oxo-butyric acid phenyl ester

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