sodium salt of carbazole

Base Information

• Chemical Name: sodium salt of carbazole
• CAS No.: 33650-06-5
• Molecular Formula: C₁₂H₈N*Na
• Molecular Weight: 189.192
• Mol file: 33650-06-5.mol

Synonyms:sodium salt of carbazole

Chemical Property of sodium salt of carbazole

Chemical Property:

Purity/Quality:

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Technology Process of sodium salt of carbazole

There total 1 articles about sodium salt of carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9H-carbazole (86-74-8,105184-46-1,97960-57-1) → sodium salt of carbazole (33650-06-5)

Guidance literature:

With sodium t-butanolate; In benzene-d6; at 80 ℃; for 0.0833333h; Schlenk technique; Inert atmosphere;

DOI:10.1002/adsc.201500301

Reference yield: 90.0%

diphenylantimony(III) chloride (2629-47-2) + sodium salt of carbazole (33650-06-5) → (C6H5)2Sb(NC6H4C6H4) (124782-50-9)

Guidance literature:

In benzene; byproducts: NaCl; stirring Ph2SbCl and Na-salt in benzene (3 h, room temp., under N2); filtration, concn. (vac.), recrystn. (petroleum ether, 40-60°C); elem. anal.;

DOI:10.1016/S0277-5387(00)83819-X

Reference yield: 51.0%

(1,3-dicyclohexyl-2,3-dihydro-1H-benzo[d]imidazol-2-yl)copper(I) chloride + sodium salt of carbazole (33650-06-5) → (BzICy)Cu(Cbz)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

upstream raw materials:

9H-carbazole

Downstream raw materials:

9-(2-pyridyl)carbazole

2-(9H-carbazole-9-yl) acetic acid ethyl ester

9-carbazolylacetic acid

(C₆H₅)2Sb(NC₆H₄C₆H₄)